A kind of anti-radiation antibacterial fabric
An antibacterial fabric and radiation protection technology, applied in textile, yarn, single-component polyester rayon, etc., can solve the problems of high cost, low radiation protection effect, complicated process, etc., and achieve the improvement of radiation protection performance. Antibacterial and anti-radiation properties, excellent antibacterial properties
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Embodiment 1
[0016] A radiation-proof and antibacterial fabric is prepared by interweaving warps and wefts perpendicularly to each other. The warp is a radiation-proof and anti-bacterial blended yarn, and the weft is a nylon fiber. Cotton fibers are blended in a spiral twisting manner. The diameter of the anti-radiation antibacterial blended yarn is 51-53 μm, the diameter of the nylon fiber is 46-48 μm, the warp density is 70 threads / cm, and the weft thread density is 54 threads / cm.
[0017] The preparation method of anti-radiation antibacterial fiber is as follows:
[0018] (1) 7 parts by weight of lead tungstate was dried at 55°C for 3 hours, then ball-milled for 8 minutes and added to 8 times the volume of absolute ethanol, and 0.7 parts of dodecyl trimethyl bromide was added. Ammonium, utilize the ultrasonic treatment of 46KHz for 35min, then filter and dry;
[0019] (2) Disperse 7 parts of lead tungstate obtained in step (1) into 70 parts of absolute ethanol, and then add 11 parts of...
Embodiment 2
[0024] The preparation method of anti-radiation antibacterial fiber is:
[0025] (1) 7 parts by weight of lead tungstate was dried at 55°C for 3 hours, then ball-milled for 8 minutes and added to 8 times the volume of absolute ethanol, and 0.7 parts of dodecyl trimethyl bromide was added. Ammonium, utilize the ultrasonic treatment of 46KHz for 35min, then filter and dry;
[0026] (2) Mix 7 parts of lead tungstate obtained in step (1) with 18 parts of ethylene glycol, react under the action of 0.07 part of ethylene glycol antimony at 203 ° C, 0.18 MPa, 150 rpm in a nitrogen atmosphere for 5 hours, and then add 110 parts of terephthalic acid and 8 parts of chlorogenic acid, continue to react for 3h, when the water output reaches 98% of the theoretical value, vacuumize to 68Pa, then react at 265°C for 3h, cool down, break the vacuum, and discharge;
[0027] (3) The anti-radiation antibacterial fiber is prepared by melt spinning the result of step (2), wherein the spinning temper...
Embodiment 3
[0030] The preparation method of anti-radiation antibacterial fiber is:
[0031] (1) 7 parts by weight of lead tungstate was dried at 55°C for 3 hours, then ball-milled for 8 minutes and added to 8 times the volume of absolute ethanol, and 0.7 parts of dodecyl trimethyl bromide was added. Ammonium, utilize the ultrasonic treatment of 46KHz for 35min, then filter and dry;
[0032] (2) Disperse 7 parts of lead tungstate obtained in step (1) into 70 parts of absolute ethanol, and then add 11 parts of methacrylic acid monomer, 5 parts of samarium methacrylate, 0.07 part of azobisisobutyronitrile to it , introduced nitrogen protection, then reacted at 72°C and 280rpm for 3h, cooled, filtered, dried at 63°C for 4h, then dried at 92°C for 3h, ball-milled to a particle size of 50-300nm to obtain lead tungstate-methyl Samarium-based acrylate complex;
[0033] (3) Mix 7 parts of the lead tungstate-samarium methacrylate compound obtained in step (2) with 18 parts of ethylene glycol, an...
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