Polymerization feeding optimization system and method

A technology of polymerization kettle and inlet, which is applied in the field of optimization of the feeding of the polymerization kettle, can solve the problems that the feeding time of the dispersant cannot be greatly shortened, the operation of the feeding system is cumbersome, and the production capacity of a single kettle is affected, so as to save manpower and simplify feeding. The effect of shortening the feeding procedure and shortening the time of entering the kettle

Inactive Publication Date: 2020-03-27
昊华宇航化工有限责任公司
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Problems solved by technology

In the process of metering into the kettle with metering tanks, both dispersants need to manually confirm whether the amount of residual roots before material preparation meets the requirements. The preparation of materials takes a long time and the metering tank needs to be rinsed twice during feeding of each dispersant. , which leads to a longer feeding time and affects the production capacity of the single kettle
The existing optimizations are all aimed at the feeding time of the dispersant, and most of them are optimized from the aspects of shortening the preparation time. Although a certain improvement effect can be obtained, they cannot fundamentally solve the problem of cumbersome operation of the original feeding system, and cannot be greatly improved. Significantly shorten the feeding time of dispersant

Method used

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  • Polymerization feeding optimization system and method

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Embodiment Construction

[0040] The invention discloses a polymerization feeding optimization system and method.

[0041] Such as figure 1 As shown, the polymerization feeding optimization system includes a dispersant storage tank, an initiator preparation tank 20, an initiator storage tank 21 and a polymerization kettle, and the initiator preparation tank 20 communicates with the initiator storage tank 21, the dispersant storage tank and the initiator storage tank 21 respectively connected to the polymerization kettle, the number of dispersant storage tanks is at least two, and the dispersant storage tanks are equipped with stirring reducers, which are characterized in that it also includes dispersant inlet pipelines, initiator inlet pipelines and flushing pipes The number of dispersant inlet pipelines is multiple and corresponds to the dispersant storage tank one by one; the inlet of the dispersant inlet pipeline is connected to the corresponding outlet of the dispersant storage tank, and the outlet...

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Abstract

The invention discloses a polymerization feeding optimization system and an optimization method. The polymerization feeding optimization system comprises dispersing agent kettle inlet pipelines, initiator kettle inlet pipelines and flushing pipelines; the dispersing agent kettle inlet pipelines are in on-to-one correspondence with dispersing agent storage tanks. The optimization method sequentially comprises the steps of water and monomer feeding, initiator preparation, first dispersing agent feeding, first dispersing agent mixing for 1 min and second dispersing agent feeding. According to theinvention, each dispersing agent is provided with an independent kettle inlet pipeline, and the flow of the dispersing agent is metered through a mass flow meter, so that the material preparation occupation time is reduced, the polymerization kettle feeding procedure is effectively simplified, the kettle feeding time is shortened, the single-kettle production capacity is improved, and the yield can be improved by 4.4%; meanwhile, metering, washing and process monitoring are all carried out through electronic equipment, a manual confirmation procedure in a traditional process is replaced, manpower is saved, and meanwhile the metering accuracy and the working efficiency of the whole kettle feeding process are effectively improved.

Description

technical field [0001] The invention relates to the technical field of optimization of feed to a polymerization kettle, in particular to a system and method for optimizing feed to a polymerization. Background technique [0002] At present, the feeding process of the 70m³ polymerization kettle is as follows: first add soft water and monomer, then add a dispersant A solution in order, then add another dispersant B solution, and finally add an initiator solution to start the reaction. Among them, the dispersant feeding procedure is as follows: the dispersant circulation pump first pumps the dispersant into the metering tank for weighing, and then uses the tank pump to pump the dispersant into the polymerization tank after the accumulated net content reaches the formula amount. In the process of metering into the kettle with metering tanks, both dispersants need to manually confirm whether the amount of residual roots before material preparation meets the requirements. The prepa...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J4/02B01F13/10B01F7/18
CPCB01J4/02B01F27/90B01F33/813
Inventor 徐素霞王振华郭金星郝利秦国昌邓晓鹏凌银霞张立治
Owner 昊华宇航化工有限责任公司
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