A kind of preparation method of hybrid pva film and polarizer
A hybrid, mixed dye technology, applied in optics, polarizing elements, optical elements, etc., can solve the problems of poor durability of iodine-based polarizers, unsuitable for high temperature and high humidity environment, etc., and achieve excellent polarization, good polarization and durability. High-temperature and high-humidity properties, the effect of improving the properties of high-temperature and high-humidity resistance
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Embodiment 1
[0033] A preparation method of a hybrid PVA film, the method comprises the steps:
[0034] Step S1. Washing: placing the PVA base film in a washing tank;
[0035] Step S2. Swelling: placing the cleaned PVA base film in a swelling tank containing 0.3% boric acid solution for swelling treatment;
[0036] Step S3. Dyeing: the swollen PVA base film is dipped in a dyeing tank containing a dyeing solution for dyeing treatment. The dyeing solution includes in mass percentage: dichroic mixed dye 1.92%, iodine 0.7%, potassium iodide 1.8% %, boric acid 0.1%;
[0037] Step S4. Stretching: After dyeing, the PVA film is first cleaned in the cleaning tank, and then enters the stretching tank for stretching. The stretching ratio is 4.6 times that of the PVA base film, and the stretching tank liquid is a 3% boric acid solution. The temperature of the extending bath is 52℃;
[0038] Step S5. Complementary color: the stretched PVA film is immersed in a color-compensating tank for color-compe...
Embodiment 2
[0042] A preparation method of a hybrid PVA film, the method comprises the steps:
[0043] Step S1. Washing: placing the PVA base film in a washing tank;
[0044] Step S2. swelling: placing the cleaned PVA base film in a swelling tank containing 0.5% boric acid solution for swelling treatment;
[0045] Step S3. Dyeing: the swollen PVA base film is dipped in a dyeing tank containing a dyeing solution for dyeing treatment. The dyeing solution includes, in terms of mass percentage: dichroic mixed dye 1.7%, iodine 0.85%, potassium iodide 1.65% %, boric acid 0.3%;
[0046] Step S4. Stretching: After dyeing, the PVA film is first cleaned in the cleaning tank, and then enters the stretching tank for stretching. The stretching ratio is 4.93 times that of the PVA base film, and the stretching tank liquid is a 2.8% boric acid solution. The temperature of the extending bath is 52℃;
[0047] Step S5. Complementary color: immerse the stretched PVA film in a color-compensating tank for c...
Embodiment 3
[0051] A preparation method of a hybrid PVA film, the method comprises the steps:
[0052] Step S1. Washing: placing the PVA base film in a washing tank;
[0053] Step S2. swelling: placing the cleaned PVA base film in a swelling tank containing 0.5% boric acid solution for swelling treatment;
[0054] Step S3. Dyeing: the swollen PVA base film is dipped in a dyeing tank containing a dyeing solution for dyeing treatment, and the dyeing solution includes in mass percentage: dichroic mixed dye 1.6%, iodine 0.9%, potassium iodide 1.75% %, boric acid 0.5%;
[0055] Step S4. Stretching: After dyeing, the PVA film is first cleaned in the cleaning tank, and then enters the stretching tank for stretching. The stretching ratio is 5.12 times that of the PVA base film, and the stretching tank liquid is a 3.1% boric acid solution. The temperature of the extending bath is 52℃;
[0056] Step S5. Complementary color: the stretched PVA film is immersed in a color-compensating tank for colo...
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