Preparation method and application of nano metal oxide and dimethylglyoxime nickel complex
A technology of diacetyl oxime and nano metal, which is applied in the field of preparation technology of inorganic nano materials, can solve the problems of low stability, unable to achieve super-hydrophobic effect, easy to fall off of thin films, etc., and achieves easy operation, improved degradation effect, and simple method. Effect
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Embodiment 1
[0031] In the first step, add 5mL tetra-n-butyl titanate, 1mL acetic acid and 6.5mL ethanol into the beaker, stir magnetically to form a colorless and transparent solution A;
[0032] In the second step, 0.6g of micron tubular dimethylglyoxime nickel [Ni(DMG) 2 ] dispersed in 10mL ethanol and ultrasonicated for 10min, then added to solution A to obtain red suspension B;
[0033] In the third step, add 10mL deionized water, 3mL absolute ethanol and 3mL acetic acid into the beaker, and stir magnetically to form a colorless and transparent solution C;
[0034] The fourth step is to gradually drop solution C into suspension B, continuously magnetically stir during the dropping process, and continue stirring for 30 min after the addition to form a red sol;
[0035] Step 5: After standing and aging the obtained red sol for 24 hours to obtain a red gel, transfer it to a drying oven at 105°C to dry for 36 hours to obtain red blocky solid particles;
[0036] In the sixth step, the ob...
Embodiment 2
[0039] In the first step, add 8mL tetra-n-butyl titanate, 2mL acetic acid and 10mL ethanol into a beaker, and magnetically stir to form a colorless and transparent solution A;
[0040] In the second step, 0.8g of micron tubular dimethylglyoxime nickel [Ni(DMG) 2 ] dispersed in 15mL ethanol and ultrasonicated for 10min, then added to solution A to obtain red suspension B;
[0041] In the third step, add 10mL deionized water, 3mL absolute ethanol and 3mL acetic acid into the beaker, and stir magnetically to form a colorless and transparent solution C;
[0042] The fourth step is to gradually drop solution C into suspension B, continuously magnetically stir during the dropping process, and continue stirring for 1 h after the addition to form a red sol;
[0043] The fifth step is to leave the obtained red sol to age for 28 hours to obtain a red gel, then transfer it to a drying oven at 100°C to dry for 40 hours to obtain red blocky solid particles;
[0044] In the sixth step, th...
Embodiment 3
[0047] In the first step, add 10mL tetra-n-butyl titanate, 2mL acetic acid and 10mL ethanol into the beaker, stir magnetically to form a colorless and transparent solution A;
[0048] In the second step, 1.0 g of micron tubular dimethylglyoxime nickel [Ni(DMG) 2 ] dispersed in 20mL ethanol and ultrasonicated for 10min, then added to solution A to obtain red suspension B;
[0049] In the third step, add 10mL deionized water, 3mL absolute ethanol and 3mL acetic acid into the beaker, and stir magnetically to form a colorless and transparent solution C;
[0050] The fourth step is to gradually drop the solution C into the suspension B, continuously magnetically stir during the dropping process, and continue to stir for 2 hours after the addition to form a red sol;
[0051] The fifth step is to leave the obtained red sol to age for 24 hours to obtain a red gel, then transfer it to a drying oven at 110°C for 30 hours to obtain a red blocky solid particle;
[0052] In the sixth ste...
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