A kind of α-glucosidase inhibitor and its application
A technology of glucosidase and inhibitor, which is applied in the field of medicine to achieve the effects of significantly inhibiting activity, improving selectivity, and enhancing drug efficacy
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Embodiment 1
[0042] Embodiment 1 of the present invention is: an α-glucosidase inhibitor, the active ingredient of which is 3-cinnamoyl-coumarin (3-cinnamoyl-2H-chromen-2-one), whose structural formula as follows: (labeled 3a).
[0043] Prepared with reference to the above steps, in the formula, R is The yield was 51.7%, and the obtained product was in the form of a yellow solid, and its structure was characterized by nuclear magnetic resonance (Nuclear Magnetic Resonance, NMR), and the results were as follows: 1 H NMR (500MHz, CDCl 3 )δ8.60(s,1H),7.92(dd,J=40,20Hz,2H),7.71-7.65(m,4H),7.44-7.39(m,4H),7.35(t,J=8,7.5 Hz,1H).
[0044] Embodiment 2 of the present invention is: an α-glucosidase inhibitor whose active ingredient is (E)-3-((p-tolyl)acryloyl)-coumarin ((E)-3-(3 -(p-tolyl)acryloyl)-2H-chromen-2-one), labeled 3b.
[0045] Prepared with reference to the above steps, in the formula, R is Its productive rate is 45.9%; The product obtained is a yellow solid, and its structure ...
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