R-T-B series magnetic material and preparation method thereof

A R-T-B, magnetic material technology, applied in the direction of magnetic materials, magnetic objects, inductor/transformer/magnet manufacturing, etc., can solve the problems of no significant improvement, high cost, limited improvement, etc.

Inactive Publication Date: 2020-08-28
FUJIAN CHANGJIANG GOLDEN DRAGON RARE EARTH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although there are a few reports in the prior art that substituting part of praseodymium for neodymium can improve the performance of magnet materials, the degree of improvement is limited and there is still no significant improveme

Method used

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  • R-T-B series magnetic material and preparation method thereof
  • R-T-B series magnetic material and preparation method thereof
  • R-T-B series magnetic material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1～19

[0160] Table 1 Formula (wt%) of R-T-B series magnetic material

[0161]

[0162]

[0163] The formula shown in Table 1 is used as a raw material, and the following preparation process is adopted to prepare the materials of Examples 1-19:

[0164] (1) Melting process: According to the formula shown in Table 1, take 50-500 kg of the prepared raw materials, put them into a crucible made of alumina, and heat them in a high-frequency vacuum induction melting furnace at 5×10 -2 Vacuum melting is carried out at 1400-1500°C in a vacuum of Pa.

[0165] (2) Casting process: after vacuum smelting, Ar gas is passed into the smelting furnace to make the air pressure reach 55,000 Pa, and then casting is carried out at 10 2 ℃ / sec-10 4 °C / sec cooling rate to obtain quenched alloy.

[0166] (3) Hydrogen crushing process: At 20-25°C, vacuumize the hydrogen crushing furnace where the quenched alloy is placed 5×10 -2 Pa, and then feed hydrogen gas with a purity of 99.9% into the hydroge...

Embodiment 1

[0183] The material that embodiment 1 makes carries out FE-EPMA detection, wherein the distribution of each element sees figure 1 .

[0184] The vertical orientation planes of Examples 1 to 19 are as follows figure 2 Shown (the two-phase particles are Pr in the Fcc phase, and the three-phase particles are Pr(Ti / Nb / Zr)B in the Dhcp phase 2 ), figure 2 The results of the FE-EPMA single-point quantitative analysis of each position are as described in Table 4:

[0185] Table 4

[0186]

[0187] Points 1 to 3 mean that three points were measured at similar positions of the same phase (for example, three grain boundary phases were measured, and three grain boundary intersections were measured).

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Abstract

The invention discloses an R-T-B series magnetic material and a preparation method thereof. The R-T-B series magnetic material provided by the invention comprises the following components (1) to (6) in percentage by weight: (1) 29.50wt.% to 33.00wt.% of R, wherein R is a rare earth element and comprises Pr and RH, Pr is greater than or equal to 15.00wt.%, and RH comprises Tb and/or Dy; (2) 0.24wt.% to 0.80wt.% of Cu; (3) 0.05wt.% to 0.50wt.% of Ti, and/or 0.10wt.% to 1.20wt.% of Nb; (4) 0wt.% to 1.52wt.% of Al; (5) 0.90wt.% to 1.03wt.% of B; and (6) 0.05wt.% to 1.50wt.% of Ga. The material hasgood residual magnetism, coercive force and the like.

Description

technical field [0001] The invention relates to an R-T-B series magnetic material and a preparation method thereof. Background technique [0002] Take Nd 2 Fe 14 Neodymium-iron-boron (NdFeB) magnet material with B as the main component has high remanence, coercive force and maximum magnetic energy product, and excellent comprehensive magnetic properties. It is used in wind power generation, new energy vehicles, and frequency conversion home appliances. The rare earth components in the current NdFeB magnet materials in the prior art are usually mainly neodymium, with only a small amount of praseodymium. Although there are a few reports in the prior art that substituting part of praseodymium for neodymium can improve the performance of magnet materials, the degree of improvement is limited and there is still no significant improvement. On the other hand, the NdFeB magnet materials with better coercive force and remanent magnetism in the prior art also need to rely on the ad...

Claims

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Application Information

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IPC IPC(8): H01F1/057H01F41/02C22C33/02C22C38/00C22C38/06C22C38/10C22C38/12C22C38/14C22C38/16
CPCC22C33/0278C22C38/002C22C38/005C22C38/06C22C38/10C22C38/12C22C38/14C22C38/16H01F1/0576H01F1/0577H01F41/0253H01F41/0266H01F41/0293
Inventor 付刚黄佳莹黄清芳许德钦
Owner FUJIAN CHANGJIANG GOLDEN DRAGON RARE EARTH CO LTD
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