A kind of high-performance solid buoyancy material and preparation method thereof
A solid buoyancy, high-performance technology, applied in the field of buoyancy materials, can solve the problems of reducing the performance of solid buoyancy material products and the damage of hollow glass beads
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0028] The present invention provides a kind of preparation method of high-performance solid buoyancy material described in the above-mentioned technical scheme, comprises the following steps:
[0029] a) mixing dicyclopentadiene, ruthenium carbene complex catalyst, silane coupling agent and polymerization inhibitor to obtain a mixture;
[0030] b) adding hollow glass microspheres to the mixture and stirring to obtain a liquid buoyant material;
[0031] c) Vibrating the liquid buoyancy material for 5min to 24h, so that the material is divided into three layers, the bottom layer is the sinking glass beads, the middle layer is the redundant liquid material and the upper layer is the intact glass bead material containing close packing;
[0032] d1) heating and solidifying the layered material, and cutting off the bottom layer and the middle layer material to obtain a high-performance solid buoyancy material;
[0033] Or d2) after discharging the bottom layer and the middle layer...
Embodiment 1
[0043] 1) Introduce 18kg of dicyclopentadiene, 0.4kg of ruthenium carbene complex catalyst, 0.2kg of trimethoxysilane coupling agent and 2kg of acetone into a mixer, and stir evenly in a vacuum environment.
[0044] 2) 4 kg of hollow glass microspheres with a true density of 0.15 g / cc, a crush strength of 2.0 MPa, and a median diameter (D50) of 50 to 60 microns are introduced into a mixer, and prepared in step 1) under a vacuum environment The liquid components are stirred well.
[0045] 3) The liquid buoyancy material prepared in step 2) is introduced into a mold whose internal dimensions are 400mm wide, 500mm long, and 300mm high; the mold is placed on a vibrating platform and vibrated at a frequency of 1 Hz for 30 minutes.
[0046] 4) Move the mold into an oven, heat it to 60°C and keep it warm for 6 hours to volatilize the acetone; then heat it to 120°C and keep it warm for 3 hours to completely cure the material.
[0047] 5) Take the cured buoyant material out of the mol...
Embodiment 2
[0051] 1) Introduce 100kg of dicyclopentadiene, 1.7kg of ruthenium carbene complex catalyst, 1.0kg of tetrakis(2-methoxyethoxy)silane coupling agent and 70kg of styrene into a mixer, and stir evenly in a vacuum environment.
[0052] 2) 110kg of hollow glass microspheres with a true density of 0.46g / cc, a crushing strength of 110MPa, and a median diameter (D50) of 15 to 30 microns are introduced into the mixer, and prepared in step 1) under a vacuum environment Stir liquid components until smooth.
[0053] The liquid buoyancy material obtained in step 2) is imported into a mold whose internal dimensions are 800mm wide, 1200mm long, and 600mm high; the bottom of the mold has a through hole, and the through hole is connected with a valve;
[0054] 3) Place the mold on a vibrating platform and vibrate at a frequency of 15 Hz for 12 hours.
[0055] 4) Open the valve at the bottom of the mold to discharge the sinking damaged glass beads and excess liquid material.
[0056] 5) Move...
PUM
| Property | Measurement | Unit |
|---|---|---|
| diameter | aaaaa | aaaaa |
| density | aaaaa | aaaaa |
| compressive strength | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More