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A vacuum heat treatment method for ultra-high toughness, medium strength and high plasticity tc32 titanium alloy parts

A technology of vacuum heat treatment and vacuum heat treatment furnace, which is applied in the field of metal material science and technology processing, can solve the problems that the fracture toughness and plasticity of parts cannot be further improved, cannot meet the use requirements, and cannot accurately control the cooling rate in different cooling stages, so as to improve the comprehensive Mechanical properties, ensuring the effect of precipitation and development

Active Publication Date: 2021-12-24
AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, at present, when the alloy is subjected to conventional heat treatment using a resistance furnace or a fuel furnace, such as β heat treatment or quasi-β heat treatment, the measured average value of fracture toughness can reach up to 125MPa m 1 / 2 level, but the plasticity is only about 11%, which cannot meet the requirements of use
This is mainly due to the fact that the use of resistance furnace or fuel furnace for heat treatment, on the one hand, cannot accurately control the cooling rate at different cooling stages, so that the precipitation of α-phase at the grain boundary of the brittle phase cannot be fully suppressed; When absorbing hydrogen and oxygen, these all lead to the failure of the fracture toughness and plasticity of the parts to be further improved

Method used

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  • A vacuum heat treatment method for ultra-high toughness, medium strength and high plasticity tc32 titanium alloy parts
  • A vacuum heat treatment method for ultra-high toughness, medium strength and high plasticity tc32 titanium alloy parts
  • A vacuum heat treatment method for ultra-high toughness, medium strength and high plasticity tc32 titanium alloy parts

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Example 1: Heat treatment of key structural components of a certain type of aircraft, the phase transition point of the furnace TC32 titanium alloy is 912°C.

[0023] Step 1. Put the cleaned TC32 titanium alloy parts into the vacuum heat treatment furnace. The vacuum pressure in the vacuum furnace is not greater than 6.7×10 -2 Pa;

[0024] Step 2. Use a heating rate of 0.3°C / s to raise the temperature of the TC32 titanium alloy parts to 922°C with the furnace, and then keep it warm for 55 minutes;

[0025] Step 3. After the heat preservation is completed, cool down to 902°C with the furnace at a cooling rate of 120°C / s, and then keep heat for 30 minutes;

[0026] Step 4. After the heat preservation is completed, cool down to 520°C with the furnace at a cooling rate of 0.01°C / s, and then keep heat for 360 minutes, then leave the furnace for air cooling.

[0027] Table 1 shows the test results of the mechanical properties of the key structural components of a certain ty...

Embodiment 2

[0030] Example 2: heat treatment of key structural components of a certain type of aircraft, the phase transition point of the furnace TC32 titanium alloy is 915°C.

[0031] Step 1. Put the cleaned TC32 titanium alloy parts into the vacuum heat treatment furnace. The vacuum pressure in the vacuum furnace is not greater than 6.7×10 -2 Pa;

[0032] Step 2. Use a heating rate of 0.3°C / s to raise the temperature of the TC32 titanium alloy parts to 925°C with the furnace, and then keep it warm for 70 minutes;

[0033] Step 3. After the heat preservation is completed, cool down to 905°C with the furnace at a cooling rate of 150°C / s, and then keep heat for 30 minutes;

[0034] Step 4. After the heat preservation is completed, cool down to 540°C with the furnace at a cooling rate of 0.05°C / s, and then hold the heat. The soaking time of heat preservation is 360min.

[0035] Table 2 shows the test results of the mechanical properties of the key structural components of a certain type of...

Embodiment 3

[0038] Example 3: Heat treatment of key structural components of a certain type of aircraft, the phase transition point of the furnace TC32 titanium alloy is 910°C.

[0039] Step 1. Put the cleaned TC32 titanium alloy parts into the vacuum heat treatment furnace. The vacuum pressure in the vacuum furnace is not greater than 6.7×10 -2 Pa;

[0040] Step 2. Use a heating rate of 0.3°C / s to raise the temperature of the TC32 titanium alloy parts to 920°C with the furnace, and then keep it warm for 60 minutes;

[0041] Step 3. After the heat preservation is completed, cool down to 900°C with the furnace at a cooling rate of 80°C / s, and then keep heat for 30 minutes;

[0042] Step 4. After the heat preservation is completed, cool down to 500°C with the furnace at a cooling rate of 0.001°C / s, and then hold the heat. The soaking time of heat preservation is 360min.

[0043] Table 3 shows the test results of the mechanical properties of the key structural components of a certain type ...

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Abstract

The invention belongs to the field of scientific and technological processing of metal materials, and relates to a vacuum heat treatment method for TC32 titanium alloy parts with ultra-high toughness, medium strength and high plasticity. The TC32 titanium alloy parts are put into a vacuum heat treatment furnace, and the vacuum pressure in the vacuum furnace is not greater than 6.7 ×10 ‑2 Pa; use a heating rate of 0.3°C / s to raise the temperature of the TC32 titanium alloy parts to Tβ+10°C with the furnace, and the soaking time for heat preservation is 45min to 90min; Cool the furnace to Tβ-10°C, then keep it warm, the soaking time is 25min to 35min; after the hold is over, cool it with the furnace to 500°C to 550°C at a cooling rate of 0.001°C / s to 0.1°C / s, and then keep it warm. The heat preservation and soaking time is 300min to 380min, and the furnace is air-cooled; through the vacuum heat treatment technology of rapid cooling in the cross-phase region and slow cooling in the two-phase region for TC32 titanium alloy parts, the purpose of precisely controlling the microstructure is achieved, and the TC32 titanium alloy is significantly improved. The comprehensive performance of the alloy, the fracture toughness reached 140MPa m 1 / 2 And above, the plasticity has reached 15% and above, and the strength is guaranteed to be 850MPa and above.

Description

technical field [0001] The invention belongs to the field of scientific and technical processing of metal materials, and relates to a vacuum heat treatment method for TC32 titanium alloy parts with ultra-high toughness, medium strength and high plasticity. Background technique [0002] With the development of aviation technology, the design idea of ​​aircraft structure has been continuously improved through the development process from static strength, dynamic strength, fatigue strength to fracture strength. Therefore, titanium alloy materials with high fracture toughness have been paid attention to, which has promoted the development of titanium alloy materials. Further development of application technology. With the continuous improvement of the overall performance requirements of my country's new generation of aircraft, the design allowable value of the fracture toughness value of a key structural component titanium alloy material needs to reach an ultra-high toughness of...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C14/00C22F1/18C22F1/02
Inventor 李明兵朱知寿王新南商国强祝力伟李静
Owner AVIC BEIJING INST OF AERONAUTICAL MATERIALS