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123results about How to "Guaranteed precipitation" patented technology

Glufosinate separation and purification method

The invention belongs to the field of pesticide production and particularly relates to a glufosinate separation and purification method. According to the method, the separation and purification is started when a glufosinate hydrochloride reaction solution in the steps of distilling the glufosinate hydrochloride reaction solution under reduced pressure to remove dilute hydrochloric acid, adding ammonia water to adjust the pH to maximally produce ammonium chloride, distilling under reduced pressure to remove water, adding a flotation solvent for dispersion, placing the material into a chute at specific temperature and speed, performing flotation separation according to the difference in the proportion of a principal component and subsidiary salt, removing the solvent, dissolving the material in aqueous methanol to remove trace ammonium chloride, filling ammonia gas to adjust the pH value to 8, performing centrifugation and drying to obtain a final product. The glufosinate separation and purification method uses a flotation method for separating the principal component glufosinate and an intermediate of the principal component from the subsidiary salt ammonium chloride and the aqueous methanol for purification and is high in yield, good in purity, simple in process, low in cost and is suitable for industrial production.
Owner:石家庄瑞凯化工有限公司

Water sealing fire retardance explosion venting device

The invention discloses a water sealing fire retardance explosion venting device which comprises a fire retardance device and an explosion venting machine. The fire retardance device comprises a fire retardance barrel body, an air inlet pipe, an air outlet pipe and a water filtering metal ring net. One end of the air inlet pipe is placed out of the fire retardance barrel body, the other end of the air inlet pipe extends into the fire retardance barrel body and is inserted to the position below a sealing water liquid level, and the water filtering metal ring net is arranged above the sealing water liquid level and is arranged outside the air inlet pipe in a sleeving mode. The explosion venting machine comprises an explosion venting barrel body, an exhaust pipe and an explosion venting pipe. The exhaust pipe and the explosion venting pipe are communicated with the explosion venting barrel body. The fire retardance barrel body is communicated with the explosion venting barrel body through the air outlet pipe and a communication pipe arranged at the bottom. An explosion piece is arranged in the explosion venting pipe. An air outlet end pipe opening of the air inlet pipe is sealed. An exhaust hole is formed in the side wall, placed below the sealing water liquid level, of the air inlet pipe. The exhaust hole is connected with an air guiding pipe. Air guiding holes for air discharging are distributed in the air guiding pipe. The instability and the acute fluctuation of the liquid level caused when air is discharged from the device exhaust pipe can be avoided, water level control is convenient, and the safety and the reliability of the device are improved.
Owner:CHINA COAL TECH & ENG GRP CHONGQING RES INST CO LTD

Preparation method of low-alloy high-strength steel plate with low residual stress

The invention relates to a preparation method of a low-alloy high-strength steel plate with low residual stress. The preparation method comprises the following steps: smelting; performing continuous casting; heating; performing rough rolling; performing refined rolling; performing laminar flow cooling; coiling; flattening; straightening; tempering; and performing cross cutting. In the heating step, the heating temperature is more than 1200 DEG C; in the refined rolling step, the final rolling temperature is 800 DEG C to 900 DEG C; in the coiling step, the rolling temperature is 550 DEG C to 650 DEG C; and in the tempering step, the tempering temperature is 550 DEG C to 650 DEG C, and the tempering heat insulation time is 10 minutes to 20 minutes. The method is applied to the steel plate which is prepared from the following chemical components: 0.04 percent to 0.12 percent of C, 0.10 percent to 0.80 percent of Si, 1.3 percent to 2.1 percent of Mn, 0 percent to 0.06 percent of Nb, 0.0 to 0.6 percent of Mo, 0 percent to 0.10 percent of V, 0.02 percent to 0.20 percent of Ti, 0.01 percent to 0.06 percent of Al, less than or equal to 0.003 percent of B, less than or equal to 0.010 percent of P, less than or equal to 0.004 percent of S, less than or equal to 0.008 percent of N, and the balance of Fe and inevitable impurities.
Owner:SHOUGANG CORPORATION +1

Production process of glutamic acid and monosodium glutamate

The invention discloses a production process of glutamic acid and monosodium glutamate, which comprises the following steps: firstly, evaporating and concentrating fermentation liquid; after concentrated sulfuric acid is added for isoelectric operation, cooling to 5-15 DEG C; obtaining an alpha-crystalline glutamic acid crystal suspension after primary separation, primary crystal washing, secondary separation and secondary crystal washing; regulating the pH value to be 4.0-5.0 at 80-90 DEG C, cooling to 35 DEG C, and obtaining a beta-crystalline glutamic acid crystal through filtration and separation, wherein the beta-crystalline glutamic acid crystal can be dried by air flow to obtain glutamic acid products, and the beta-crystalline glutamic acid crystal can be continuously neutralized and refined to obtain monosodium glutamate products; carrying out cyclone precipitation on primary mother liquid after primary separation, removing protein in supernatant liquid by flocculation air flotation process, and drying the protein to obtain bacterial protein powder; and carrying out ion exchange on the deproteinized clear liquid to prepare compound fertilizer. The extraction method of the glutamic acid provided by the invention fundamentally reduces the generation of waste water, improves the extraction yield and the product quality, reduces the amount of water for exchanging ions and washing columns to the minimum, and has higher production efficiency and lower production cost.
Owner:BEIJING PIHUA BIOLOGICAL TECH

A kind of method utilizing potassium mixed salt to prepare potassium chloride

The invention discloses a method for preparing potassium chloride from potassium mixed salt. The method comprises the steps that the potassium mixed salt is dissolved in water, solid-liquid separation is carried out, and a potassium mixed salt solution is obtained; a first-section nanofiltration step is carried out, wherein a nanofiltration membrane system is adopted for carrying out first-section nanofiltration treatment on the potassium mixed salt solution, first-section concentrated water and first-section produced water are obtained, the nanofiltration system comprises a first nanofiltration membrane assembly, a first concentrated water box and a first produced water box, and the first concentrated water box and the first produced water box are connected to the first nanofiltration membrane assembly; the first-section concentrated water is stored in the first concentrated water box, and the first-section produced water is stored in the first produced water box; the first-section produced water is subjected to evaporative crystallization, and sylvinite ore is obtained; the sylvinite ore is subjected to flash melting crystallization, and potassium chloride is obtained. The novel method is used for producing potassium chloride from the potassium mixed salt and has the advantages of being simple in process, high in product purity, large in particle and high in yield.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI

Utilize potassium mixed salt to prepare the method for potassium chloride

The invention discloses a method for preparing potassium chloride by utilizing potassium mixed salt. The method comprises the steps that a reverse flotation process is adopted to remove sodium chloride in the potassium mixed salt, and a tailing is obtained; the tailing is dissolved in water, and solid-liquid separation is performed to obtain a tailing solution; a section of nanofiltration step is executed, wherein a nanofiltration membrane system is adopted to conduct a section of nanofiltration treatment on the tailing solution to obtain a section of concentrated water and a section of produced water and comprises a first nanofiltration membrane module and a first concentrated water tank and a first produced water tank connected to the first nanofiltration membrane module, the section of concentrated water is stored in the first concentrated water tank, and the section of produced water is stored in the first produced water tank; evaporative crystallization is conducted on the section of produced water to obtain the potassium chloride. The invention provides a novel method for producing potassium chloride by using potassium mixed salt as a raw material. The method has the advantages of being simple in process, high in product purity and high in yield.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI

Novel pulverized coal high-pressure forming device

The invention relates to the technical field of a pulverized coal forming device, and discloses a novel pulverized coal high-pressure forming device. The novel pulverized coal high-pressure forming device comprises a first conveying device, a screening box with a feeding port at the lower portion of the right side, a first screen mesh, a conveying channel, a first lifting device, a second liftingdevice, a supporting plate, a pulverizing hydraulic rod, a pulverizing hammer, a second screen mesh, a second conveying device, a screw pressing device, an electric heating layer, a steam exhaust portand a molding device; pulverized coal is screened and smashed through the screening device, when the size of a molded product needs to be changed, a left adjusting hydraulic rod and a right adjustinghydraulic rod are adjusted to move a left adjusting plate and a right adjusting plate in the same or opposite direction, and extrusion molding products in different sizes are achieved; and the novelpulverized coal high-pressure forming device solves the problem that according to an existing pulverized coal forming device, the pulverized coal contains irregular pulverized coal particles or large-volume pulverized coal briquettes, consequently the compactness of the pulverized coal products is insufficient, the strength is not high, and diversified production of the pulverized coal forming products cannot be achieved.
Owner:XINJIANG JIEJING ENERGY TECH RES INST
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