A refinement process for methyl cellulose
A technology of methyl cellulose and ethyl cellulose, which is applied in the field of material labeling, can solve problems such as unstable performance of methyl cellulose, improve water retention and adhesion, increase particle size, and improve particle size distribution uniform effect
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Embodiment 1
[0016] A refinement process for methyl cellulose, comprising the steps of:
[0017] Step 1, adding methyl cellulose to 1L of ethanol aqueous solution and stirring evenly, filtering to obtain a solution, the concentration of the methyl cellulose in the ethanol aqueous solution is 100g / L, and the ethanol volume content in the ethanol aqueous solution is 30%;
[0018] Step 2, adding ethyl cellulose to the dissolving solution and stirring evenly to obtain a mixed dissolving solution, then spraying the mixed dissolving solution evenly in the reaction kettle, standing and settling at a constant temperature, and blowing the tail with hot nitrogen to obtain mixed cellulose particles; wherein , the addition of ethyl cellulose is 20% of the mass of methyl cellulose, the spray volume of uniform spray is 4mL / min, and the spray area is 10cm 2 , the temperature of standing at constant temperature is 100°C; the temperature of hot nitrogen is 100°C;
[0019] Step 3: Add the mixed cellulose ...
Embodiment 2
[0023] A refinement process for methyl cellulose, comprising the steps of:
[0024] Step 1, adding methyl cellulose to 1L ethanol aqueous solution and stirring evenly, filtering to obtain a solution, the concentration of the methyl cellulose in the ethanol aqueous solution is 200g / L, and the volume content of ethanol in the ethanol aqueous solution is 50 %;
[0025] Step 2, adding ethyl cellulose to the dissolving solution and stirring evenly to obtain a mixed dissolving solution, then spraying the mixed dissolving solution evenly in the reaction kettle, standing and settling at a constant temperature, and blowing the tail with hot nitrogen to obtain mixed cellulose particles; wherein , the addition of ethyl cellulose is 30% of the mass of methyl cellulose, the spray volume of uniform spray is 8mL / min, and the spray area is 30cm 2 , the temperature of standing at constant temperature is 120°C; the temperature of hot nitrogen is 110°C;
[0026] Step 3: Add the mixed cellulose...
Embodiment 3
[0030] A refinement process for methyl cellulose, comprising the steps of:
[0031] Step 1, adding methyl cellulose to 1L ethanol aqueous solution and stirring evenly, filtering to obtain a solution, the concentration of the methyl cellulose in the ethanol aqueous solution is 150g / L, and the ethanol volume content in the ethanol aqueous solution is 40 %;
[0032] Step 2, adding ethyl cellulose to the dissolving solution and stirring evenly to obtain a mixed dissolving solution, then spraying the mixed dissolving solution evenly in the reaction kettle, standing and settling at a constant temperature, and blowing the tail with hot nitrogen to obtain mixed cellulose particles; wherein , the addition of ethyl cellulose is 25% of the mass of methyl cellulose, the spray volume of uniform spray is 6mL / min, and the spray area is 20cm 2 , the temperature of standing at constant temperature is 110°C; the temperature of hot nitrogen is 105°C;
[0033] Step 3: Add the mixed cellulose pa...
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