A refinement process for methyl cellulose

A technology of methyl cellulose and ethyl cellulose, which is applied in the field of material labeling, can solve problems such as unstable performance of methyl cellulose, improve water retention and adhesion, increase particle size, and improve particle size distribution uniform effect

Active Publication Date: 2022-03-08
RICOH THERMAL MEDIA WUXI CO
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Aiming at the problems in the prior art, the present invention provides a thinning process of methyl cellulose, which solves the problem of unstable performance of methyl cellulose, and uses spray solidification combined with expansion and crushing to achieve the effect of further crushing and realize Further decrease in particle size, increase the particle size and uniform particle size distribution of methyl cellulose

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] A refinement process for methyl cellulose, comprising the steps of:

[0017] Step 1, adding methyl cellulose to 1L of ethanol aqueous solution and stirring evenly, filtering to obtain a solution, the concentration of the methyl cellulose in the ethanol aqueous solution is 100g / L, and the ethanol volume content in the ethanol aqueous solution is 30%;

[0018] Step 2, adding ethyl cellulose to the dissolving solution and stirring evenly to obtain a mixed dissolving solution, then spraying the mixed dissolving solution evenly in the reaction kettle, standing and settling at a constant temperature, and blowing the tail with hot nitrogen to obtain mixed cellulose particles; wherein , the addition of ethyl cellulose is 20% of the mass of methyl cellulose, the spray volume of uniform spray is 4mL / min, and the spray area is 10cm 2 , the temperature of standing at constant temperature is 100°C; the temperature of hot nitrogen is 100°C;

[0019] Step 3: Add the mixed cellulose ...

Embodiment 2

[0023] A refinement process for methyl cellulose, comprising the steps of:

[0024] Step 1, adding methyl cellulose to 1L ethanol aqueous solution and stirring evenly, filtering to obtain a solution, the concentration of the methyl cellulose in the ethanol aqueous solution is 200g / L, and the volume content of ethanol in the ethanol aqueous solution is 50 %;

[0025] Step 2, adding ethyl cellulose to the dissolving solution and stirring evenly to obtain a mixed dissolving solution, then spraying the mixed dissolving solution evenly in the reaction kettle, standing and settling at a constant temperature, and blowing the tail with hot nitrogen to obtain mixed cellulose particles; wherein , the addition of ethyl cellulose is 30% of the mass of methyl cellulose, the spray volume of uniform spray is 8mL / min, and the spray area is 30cm 2 , the temperature of standing at constant temperature is 120°C; the temperature of hot nitrogen is 110°C;

[0026] Step 3: Add the mixed cellulose...

Embodiment 3

[0030] A refinement process for methyl cellulose, comprising the steps of:

[0031] Step 1, adding methyl cellulose to 1L ethanol aqueous solution and stirring evenly, filtering to obtain a solution, the concentration of the methyl cellulose in the ethanol aqueous solution is 150g / L, and the ethanol volume content in the ethanol aqueous solution is 40 %;

[0032] Step 2, adding ethyl cellulose to the dissolving solution and stirring evenly to obtain a mixed dissolving solution, then spraying the mixed dissolving solution evenly in the reaction kettle, standing and settling at a constant temperature, and blowing the tail with hot nitrogen to obtain mixed cellulose particles; wherein , the addition of ethyl cellulose is 25% of the mass of methyl cellulose, the spray volume of uniform spray is 6mL / min, and the spray area is 20cm 2 , the temperature of standing at constant temperature is 110°C; the temperature of hot nitrogen is 105°C;

[0033] Step 3: Add the mixed cellulose pa...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
particle diameteraaaaaaaaaa
particle diameteraaaaaaaaaa
Login to view more

Abstract

The invention discloses a refinement process of methyl cellulose, which comprises: adding methyl cellulose to ethanol aqueous solution and stirring evenly, and filtering to obtain a solution; adding ethyl cellulose to the solution and stirring evenly to obtain a mixed Then spray the mixed solution evenly in the reaction kettle, let it settle at a constant temperature, and blow off the tail with hot nitrogen to obtain mixed cellulose particles; add the mixed cellulose particles to ethylbenzene and stir evenly, filter and air-dry until the surface is dry , to obtain porous methylcellulose particles, and then spray water mist on the surface to make the surface of methylcellulose sticky, and dry to obtain wrapped methylcellulose; add wrapped methylcellulose into a sealed reaction kettle, pressurize at constant temperature 10-30min, constant temperature and pressure relief to obtain crushed methyl cellulose. The invention solves the problem of unstable performance of the methyl cellulose, uses spray solidification combined with expansion and crushing to realize further reduction of the particle size, and improves the particle size and particle size distribution uniformity of the methyl cellulose.

Description

technical field [0001] The invention belongs to the field of material labels, and in particular relates to a process for refining methyl cellulose. Background technique [0002] In the production process of logistics labels, methyl cellulose is one of the most commonly used raw materials. There are various sizes of methyl cellulose on the market, and there are certain differences in the production processes adopted by different manufacturers. The purity of methyl cellulose produced There are also slight differences. Mixing them will easily lead to a decline in the quality of material labels. Contents of the invention [0003] Aiming at the problems in the prior art, the present invention provides a thinning process of methyl cellulose, which solves the problem of unstable performance of methyl cellulose, and uses spray solidification combined with expansion and crushing to achieve the effect of further crushing and realize The further reduction of the particle size increa...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Patents(China)
IPC IPC(8): C08J3/12C08L1/28
Inventor 钱泉俞海波
Owner RICOH THERMAL MEDIA WUXI CO
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products