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Traditional Chinese medicine composite antiviral multifunctional degradable polylactic acid fiber and preparation method thereof

A polylactic acid fiber, anti-virus technology, applied in the chemical characteristics of fibers, rayon manufacturing, single-component polyester rayon, etc., can solve the problem of increasing process steps and energy consumption, and the effect of functional nanoparticles cannot be effectively exerted. The fiber chips are difficult to mix and disperse uniformly, etc., to achieve good mixing and dispersing effect, good stability, and the effect of simplifying the preparation process

Active Publication Date: 2021-05-07
芯安健康科技广东有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The problems of this process are: 1. The polymer fiber material first needs to be polymerized, separated, and processed into fiber slices, and then the fiber slices and functional nanoparticles are melt-mixed and extruded. The fiber slices have undergone two molding processes, which significantly increases process steps and energy consumption
2. It is difficult to mix and disperse the formed fiber slices evenly in the process of melting and mixing with functional nanoparticles, so that the effect of functional nanoparticles cannot be effectively exerted

Method used

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  • Traditional Chinese medicine composite antiviral multifunctional degradable polylactic acid fiber and preparation method thereof
  • Traditional Chinese medicine composite antiviral multifunctional degradable polylactic acid fiber and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] The preparation method of a traditional Chinese medicine composite anti-virus, anti-bacterial, anti-mite, far-infrared multifunctional degradable polylactic acid fiber includes the following preparation steps:

[0039] (1) Fermentation and extraction of corn to obtain lactic acid, and then dehydration condensation at a temperature of 100-170°C and reduced pressure to obtain a lactic acid prepolymer;

[0040] (2) Add 95 parts by mass of lactic acid prepolymer and 5 parts by mass of traditional Chinese medicine composite antiviral, antibacterial, anti-mite far-infrared multifunctional nanoparticles and catalyst stannous octoate into a twin-screw extruder, and melt and mix at a temperature of 160-200°C polycondensation to obtain functional polylactic acid;

[0041] (3) The obtained functional polylactic acid is formed by spinning to obtain a traditional Chinese medicine compound anti-virus, anti-bacterial, anti-mite and far-infrared multifunctional degradable polylactic ac...

Embodiment 2

[0048] The preparation method of a kind of traditional Chinese medicine compound anti-virus, anti-bacterial, anti-mite, far-infrared anion multifunctional degradable polylactic acid fiber of this embodiment includes the following preparation steps:

[0049] (1) Fermentation and extraction of corn to obtain lactic acid, and then dehydration condensation at a temperature of 100-170°C and reduced pressure to obtain a lactic acid prepolymer;

[0050] (2) Add 85 parts by mass of lactic acid prepolymer and 15 parts by mass of traditional Chinese medicine composite antiviral, antibacterial, anti-mite, far-infrared negative ion multifunctional nanoparticles and catalyst stannous octoate into a twin-screw extruder, and melt at a temperature of 160-200°C Mix polycondensation to obtain functional polylactic acid;

[0051] (3) The obtained functional polylactic acid is formed by spinning to obtain a traditional Chinese medicine compound anti-virus, anti-bacterial, anti-mite and far-infrar...

Embodiment 3

[0058] The preparation method of a kind of traditional Chinese medicine composite anti-virus, anti-bacterial, anti-mite anion anion multifunctional degradable polylactic acid fiber of this embodiment comprises the following preparation steps:

[0059] (1) Fermentation and extraction of corn to obtain lactic acid, and then dehydration condensation at a temperature of 100-170°C and reduced pressure to obtain a lactic acid prepolymer;

[0060] (2) Add 90 parts by mass of lactic acid prepolymer and 10 parts by mass of traditional Chinese medicine composite antiviral, antibacterial, anti-mite anion multifunctional nanoparticles and catalyst stannous octoate into a twin-screw extruder, melt, mix and polycondense at a temperature of 160-200°C , to obtain functional polylactic acid;

[0061] (3) The obtained functional polylactic acid is formed by spinning to obtain a traditional Chinese medicine compound anti-virus, anti-bacterial, anti-mite and far-infrared multifunctional degradabl...

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Abstract

The invention belongs to the field of functional fiber materials, and discloses a traditional Chinese medicine composite antiviral multifunctional degradable polylactic acid fiber and a preparation method thereof. The preparation method comprises the following steps of fermenting a starch fermentation raw material to extract lactic acid, performing dehydration condensation to obtain a lactic acid prepolymer, adding the lactic acid prepolymer, functional nanoparticles and a catalyst into an extruder, performing melt mixing polycondensation to obtain functional polylactic acid, and performing spinning molding to obtain a product. The functional nanoparticles are obtained by adsorbing traditional Chinese medicine antiviral components by an inorganic nano powder material subjected to surface modification by porous silicon dioxide and a silane coupling agent. Functional modification of the polylactic acid fiber and upstream fiber polymerization are effectively coupled, so that the process steps are remarkably simplified, the production energy consumption is reduced, and better mixing and dispersing effects and stability are achieved. Meanwhile, an inorganic antibacterial health-care function and a traditional Chinese medicine antiviral function are integrated into the same particle, so that the antibacterial, antiviral and health-care functions can be played at the same time. The obtained functional fiber has the advantages of environmental protection, degradability and cyclic regeneration.

Description

technical field [0001] The invention belongs to the field of functional fiber materials, and in particular relates to a traditional Chinese medicine composite anti-virus multifunctional degradable polylactic acid fiber and a preparation method thereof. Background technique [0002] Polylactic acid fiber is made from starch-containing agricultural products such as corn, wheat, and sugar beet. After fermentation to generate lactic acid, it is made by polycondensation and melt spinning. . Polylactic acid fiber is a kind of synthetic fiber whose raw material can be planted, is easy to plant, and the waste can be degraded naturally in nature. It can be decomposed into carbon dioxide and water by microorganisms in soil or seawater. When burned, it will not emit poisonous gas and cause pollution. It is a sustainable ecological fiber. The fabric has good handle and drapability, anti-ultraviolet radiation, low flammability and excellent processing performance. It is suitable for var...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/92D01F1/10
CPCD01F1/10D01F1/103D01F6/92
Inventor 黄钊维邓细利罗湘军钟敏丽黄蕊烨
Owner 芯安健康科技广东有限公司
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