Silica gel for wine bottle cap and preparation method thereof, and wine bottle cap
A wine bottle cap and silica gel technology, applied in the field of silica gel, can solve the problems of easy deformation and shedding under force, and achieve the effects of not easily deformed and detached, reducing the possibility of deformation and shedding under force, and excellent sealing.
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preparation example 1
[0035] Add 1 mol of trimethylolpropane triacrylate to the three-necked flask equipped with a dropping funnel, react in an ice-water bath environment, and slowly add 1 mol of diethanolamine dropwise with a dropping funnel under stirring at a rotating speed of 180 r / min. Continue to react for 5h, when the infrared absorption spectrum is 3350cm -1 The N-H peak at the position disappeared, which proved that the reaction was completed and an active amine co-initiator was obtained.
[0036] Preparation example of modifier
preparation example 2
[0038] A method for preparing a modifier. At 25° C., 1kg of tripropylene glycol diacrylate and 0.08kg of an ultraviolet photoinitiator are added to a reaction kettle, and mixed uniformly to obtain a modifier, wherein the ultraviolet photoinitiator is benzene formyl formate.
preparation example 3
[0040] A preparation method of a modifier is different from Preparation Example 2 in that the additions of tripropylene glycol diacrylate and benzoyl formate are 1.05kg and 0.11kg, respectively.
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