Weeding composition containing propanil and tembotrions
A herbicidal composition and a technology of cyclosulfonone are applied in the field of pesticides, and can solve the problems of rolling loss and impermeability of pharmaceuticals
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Embodiment 1
[0042] This embodiment is a herbicidal composition containing propanil and tembotrione, comprising the following components in parts by weight:
[0043] 20 parts of propanil, 10 parts of tembotrione, 20 parts of filler or solvent, 5 parts of penetrant, and 5 parts of defoamer;
[0044] Wherein the penetrant is prepared by the following steps:
[0045] S1: Add phenylpropionic acid to a three-necked flask, add catalyst, and toluene as a solvent, grind trichloromethyl carbonate and add it to a three-necked flask, control the temperature at 20°C, stir for 5 minutes, raise the temperature to 60°C, and control the heating rate 3°C / min, reacted for 4h, and distilled under reduced pressure to obtain intermediate A;
[0046] S2: Add dichloromethane as a solvent to a three-necked flask, add eugenol, 4-dimethylaminopyridine and triethylamine, stir mechanically at 300r / min, control the system temperature in an ice-water bath at 0°C, add intermediate A dropwise, and control The dropping ...
Embodiment 2
[0054] This embodiment is a herbicidal composition containing propanil and tembotrione, comprising the following components in parts by weight:
[0055] 20 parts of propanil, 20 parts of tembotrione, 30 parts of filler or solvent, 6 parts of penetrant, and 5 parts of defoamer;
[0056] Wherein the penetrant is prepared by the following steps:
[0057] S1: Add phenylpropionic acid to a three-necked flask, add catalyst, and toluene as a solvent, grind trichloromethyl carbonate and add it to a three-necked flask, control the temperature at 20°C, stir for 5 minutes, raise the temperature to 60°C, and control the heating rate 3°C / min, reacted for 4h, and distilled under reduced pressure to obtain intermediate A;
[0058] S2: Add dichloromethane as a solvent to a three-necked flask, add eugenol, 4-dimethylaminopyridine and triethylamine, stir mechanically at 300r / min, control the system temperature in an ice-water bath at 0°C, add intermediate A dropwise, and control The dropping ...
Embodiment 3
[0066] This embodiment is a herbicidal composition containing propanil and tembotrione, comprising the following components in parts by weight:
[0067] 40 parts of propanil, 20 parts of tembotrione, 30 parts of filler or solvent, 5 parts of penetrant, and 6 parts of defoamer;
[0068] Wherein the penetrant is prepared by the following steps:
[0069] S1: Add phenylpropionic acid to a three-necked flask, add catalyst, toluene as a solvent, grind trichloromethyl carbonate into a three-necked flask, control the temperature at 25°C, stir for 15 minutes, raise the temperature to 65°C, and control the heating rate 5°C / min, react for 5h, and distill under reduced pressure to obtain intermediate A;
[0070] S2: Add dichloromethane as a solvent to a three-necked flask, add eugenol, 4-dimethylaminopyridine and triethylamine, mechanically stir at 350r / min, control the temperature of the system in an ice-water bath at 6°C, add intermediate A dropwise, and control The dropping rate was ...
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