Environment-friendly degradable sampling swab and preparation method thereof
An environmentally friendly, swab-based technology, which can solve problems such as damage and environmental pollution by removing certain components and weighing, using stable tension/pressure to test material strength, and testing wear resistance.
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preparation example I-1
[0041] A modified pomelo peel fiber, which is prepared by the following method:
[0042] Step S1: Take 170kg of grapefruit peel, remove impurities, peel off the outer skin of grapefruit peel, then collect white flocs, place them in 40wt% NaOH solution and soak for 30min, the surface of NaOH solution is submerged in grapefruit peel, take it out, and rinse with water 5 times, dried, and ground to 100 mesh to obtain pomelo peel particles;
[0043] Step S2: Add 270kg of n-hexane into the reaction kettle, then add pomelo peel particles into the reaction kettle, then add 50kg of acrylic acid and 1kg of 98wt% concentrated sulfuric acid in sequence, mix well, heat up to 70°C, and reflux for 10h;
[0044] Step S3: Filtrate, take the filter residue, place the filter residue in n-hexane with a volume ratio of 1:10, ultrasonicate for 15 minutes, repeat the above operation four times in step S3, dry, and spin to obtain modified pomelo peel fiber.
preparation example I-2
[0046] A modified pomelo peel fiber, which differs from Preparation I-1 in that an equal amount of acetoacetic acid is used to replace acrylic acid, and the rest are the same as Preparation I-1.
preparation example II-1
[0049] A kind of microcrystalline cellulose modified polylactic acid, it adopts following method to prepare:
[0050] 120kg of polylactic acid, 25kg of microcrystalline cellulose, and 7kg of hydroxypropyl starch were added to a twin-screw extruder, melt-extruded and granulated to obtain modified polylactic acid, and the temperature of the machine head was 160°C.
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