Tech of sintering Nb2O5-TiO2 system deelectric ceramic
A technology of nb2o5-tio2 and dielectric ceramics, which is applied in the field of dielectric ceramics preparation, can solve the problems of long holding time, low dielectric coefficient, and long preparation cycle, etc., and achieve the goals of increased production efficiency, reduced energy consumption, and shortened preparation cycle Effect
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Embodiment 1
[0019] Example 1: The Nb 2 O 5 And TiO 2 Powder according to the proportion (Nb 2 O 5 ) 0.95 (TiO 2 ) 0.05 Batching, mechanical ball milling for 12 hours, drying; heating up to 1250°C at a rate of 200°C / hour for pre-sintering and keeping the temperature for 18 hours. The pre-fired powder is mechanically ball milled for 12 hours and dried; the pre-fired powder will be mixed with 3% mass concentration of polyvinyl alcohol (PVA) glue for granulation, where the weight of the glue is the powder 6% of the total weight; under a pressure of 200 MPa, press into a green sheet; heat the green body at a rate of 100°C / hour to 1380°C for sintering, keep it for 2 hours, and then reduce to room temperature at a rate of 150°C / hour, Finally sintered into a dense flake ceramic body; gold electrodes were sprayed on the upper and lower surfaces of the ceramic sheet, and the dielectric properties were measured with HP4284ALCR precision measuring instrument under conventional measurement conditions (1MH...
Embodiment 2
[0021] Embodiment 2: Nb 2 O 5 And TiO 2 Powder according to the proportion (Nb 2 O 5 )0.92(TiO 2 ) 0.08 for batching, mechanical ball milling for 12 hours, drying; heating up to 1250°C at a rate of 200°C / hour for pre-burning, and keeping the temperature for 18 hours. The pre-fired powder is mechanically ball milled for 12 hours and dried; the pre-fired powder will be mixed with 3% mass concentration of polyvinyl alcohol (PVA) glue for granulation, where the weight of the glue is the powder 6% of the total weight; under a pressure of 200 MPa, press into a green sheet; heat the green body at a rate of 100°C / hour to 1370°C for sintering, keep it for 15 hours, and then reduce to room temperature at a rate of 150°C / hour, Finally sintered into a dense flake ceramic body; gold electrodes were sprayed on the upper and lower surfaces of the ceramic sheet, and the dielectric properties were measured with HP4284ALCR precision measuring instrument under conventional measurement conditions (1M...
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