The invention discloses a dual-
niobium-source
alkali metal niobate micro-nano wire material. The micro-nano wire material is synthesized through a traditional
ceramic solid-phase
sintering process byusing K2CO3, Na2CO3, Nb2O5, C10H5NbO20, BaCO3 and Bi2O3 as raw materials which are blended according to a
chemical formula of (1-y)K<z>Na<1-z>Nb<(C)x>Nb<(N)1-x>O<3-y>BaBiO<3>, wherein Nb<(C)> is an element Nb from a
niobium source C<10>H<5>NbO<20>, Nb<(N)> is an element Nb from a
niobium source Nb<2>O<5>, x is greater than 0 and less than or equal to 0.1, y is greater than 0 and less than 0.1, andz is greater than or equal to 0.4 and less than or equal to 0.6. A preparation method of the dual-niobium-source
alkali metal niobate micro-nano wire material comprises the following steps of (1) rawmaterial
drying; (2)
raw material weighing and ball-milling; (3) pre-
sintering of
powder obtained after ball-milling; (4) secondary ball-milling of pre-sintered
powder; (5) pressing of
powder obtained after secondary ball-milling into a round billet; (6) heat preservation treatment of the round billet. The dual-niobium-source
alkali metal niobate micro-nano wire material and the preparation method thereof have the advantages that after the double niobium sources are adopted, the
crystallinity of pressed billet powder and the
growth speed of micro-nano wires can be effectively increased; meanwhile,
purified water can be used as a ball-milling medium, no absolute ethyl
alcohol is needed, and thus the cost is greatly saved and environment
pollution and potential safety hazards in the dryingprocess are reduced; the pre-
sintering temperature is lowered by 150-425 DEG C, and heat preservation time is shortened.