A NiZnCu ferrite material and preparing method thereof
A ferrite material and formula technology, applied in the field of magnetic materials, can solve the problems of long pre-sintering temperature and holding time, difficult to control the weighing of ingredients, increased power consumption, etc., to achieve high magnetic permeability and Q value stability, production Good batch consistency and the effect of reducing the burn-in temperature
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Embodiment 1
[0025] Embodiment 1: by molecular formula (Ni 0.15 Zn 0.65 Cu 0.2 O)Fe 1.99 o 3 Calculated as the weighing of the oxide containing each metal ion, produce 7 batches, each batch of 100kg, each oxide powder gross weight is 99.5kg, add the organic additive stearic acid that weight is 0.1kg, use The average particle size is 1 μm after ball milling and mixing in a horizontal ball mill for 6 hours. The pre-calcination temperatures for the production of 7 batches are 650°C, 700°C, 750°C, 800°C, 850°C, 900°C, and 950°C, and the highest temperature is kept for 2 hours. After burning, add 0.4kg of organic additive stearic acid, pulverize with a horizontal ball mill for 6 hours to an average particle size of 1.4 μm, and dry to obtain finished powder. Add 1% PVA and 2% Bi to the finished powder 2 o 3 After granulation, it is pressed into a magnetic ring for testing. The green body of the magnetic ring has an outer diameter of 42 mm, an inner diameter of 30 mm, and a thickness of 4 m...
Embodiment 2
[0027] Embodiment 2: by molecular formula (Ni 0.15 Zn 0.65 Cu 0.2 O)Fe 1.99 o 3 Calculated as the weighing of the oxide containing each metal ion, 7 batches were produced, each batch was 100kg, the total weight of each oxide powder was 99.5kg, the auxiliary material was CoO with a weight of 0.1kg and the added weight was 0.1kg Stearic acid, an organic additive, was mixed with a horizontal ball mill for 6 hours and the average particle size was 1 μm. The pre-calcination temperatures of the 7 batches were 650°C, 700°C, 750°C, 800°C, 850°C, 900°C, and 950°C. ℃, heat preservation at the highest temperature for 2 hours, add 0.3 kg of organic additive stearic acid after pre-calcination, ball mill for 6 hours with a horizontal ball mill to an average particle size of 1.4 μm, and dry to obtain the finished powder. Add 1% PVA and 3% Bi to the finished powder 2 o 3 After granulation, it is pressed into a magnetic ring for testing. The green body of the magnetic ring has an outer d...
Embodiment 3
[0029] Embodiment 3: by molecular formula (Ni 0.4 Zn 0.5 Cu 0.2 O)Fe 1.97 o 3Calculated as the weight weighing of oxides containing each metal ion, 7 batches were produced, each batch was 100kg, the total weight of each oxide powder was 94kg, and the auxiliary materials were CoO and MnO with a total weight of 4kg 2 、Al 2 o 3 , SiO 2 and the organic additives stearic acid and sodium oleate with a total weight of 1 kg, mixed with a horizontal ball mill for 4 hours, the average particle size is 1 μm, and the pre-calcination temperatures of 8 batches are 600 ° C, 650 ° C, 700 ° C, and 750 ° C respectively , 800°C, 850°C, 900°C, 950°C, keep the temperature for 1.5h at the highest temperature, add organic additives stearic acid and sodium oleate with a total weight of 1kg after pre-calcination, and use a horizontal ball mill to pulverize for 6h to an average particle size of 1.4μm , and dried to obtain finished powder. Add 1% PVA and 3% Bi to the finished powder 2 o 3 Afte...
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