Technique for quick sintering ceramics in (Ta2O5)1-x(TiO2)x system
A rapid sintering and system technology, applied in the field of preparation of 1-xx system dielectric ceramics, can solve the problems of long preparation cycle, long time, and long time, and achieve the effects of shortening the preparation cycle, reducing energy consumption and improving efficiency
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[0017] What the present invention provides is a fast energy-saving sintering high dielectric constant (Ta 2 o 5 ) 1-x (TiO 2 ) x The craft of ceramics. The core part of the process is: the Ta 2 o 5 and TiO 2 Powder according to the ratio (1-x)Ta 2 o 5 :xTiO 2Do the batching within the range of x=0.01-0.13 molar ratio, then ball mill and mix for 18 hours, pre-calcine at 1200°C for 12 hours, then ball-mill the pre-fired powder for 18 hours, and dry; Concentration is after the polyvinyl alcohol (PVA) glue of 3% is mixed into powder (the weight of glue is 6% of powder gross weight), takes by weighing the powder of about 1.5-1.8 gram weight, under 200 MPa pressure, Pressed into a sheet-shaped green body with a diameter of 13mm and a thickness of 2mm; the temperature was raised to 1550°C at a rate of 100°C / hour, and kept at a temperature of 1 hour, and then lowered to room temperature at a rate of 150°C / hour, and finally sintered into a dense sheet Shaped ceramic body, it...
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