Technique for quick sintering ceramics in (Ta2O5)1-x(TiO2)x system
A rapid sintering and system technology, which is applied in the field of preparation of 1-xx system dielectric ceramics, can solve the problems of long time, long preparation cycle and long time, and achieve the effect of reducing energy consumption, shortening preparation cycle and improving efficiency
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[0016] The invention provides a fast energy-saving sintering high dielectric constant (Ta 2 O 5 ) 1-x (TiO 2 ) x Ceramic craftsmanship. The core part of the process is: the Ta 2 O 5 And TiO 2 Powder according to the proportion (1-x) Ta 2 O 5 : XTiO 2The compounding is carried out in the range of x=0.01-0.13 molar ratio, and then after 18 hours of ball milling and mixing, it is pre-fired at 1200°C for 12 hours, and then the pre-fired powder is ball milled for 18 hours and dried; After mixing the polyvinyl alcohol (PVA) glue with a concentration of 3% into the powder (the weight of the glue is 6% of the total weight of the powder), weigh about 1.5-1.8 grams of the powder, and under the pressure of 200 MPa, It is pressed into a sheet-like body with a diameter of 13mm and a thickness of 2mm; the temperature is raised to 1550°C at a rate of 100°C / hour, and the temperature is kept for 1 hour, and then it is reduced to room temperature at a rate of 150°C / hour, and finally sintered into a...
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