Fluorine removing technique pointed of newly discovered fluorine source of fluorosis at western area of Guizhou province
A fluoride reduction and fuel technology, which is applied in the petroleum industry, solid fuel, fuel and other directions, can solve the problems of fluoride poisoning improvement, influence promotion, and may not be very practical, and achieve the effect of taking into account combustion performance, easy promotion, and good fluorine fixing effect.
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[0029] Measuring principle and method:
[0030] According to the National Standard of the People’s Republic of China GB / T4633-1997 "Method for the determination of fluorine in coal": Weigh 0.5 (±0.0002) g of air-dried coal sample and 0.5 g of quartz sand, mix them in a combustion boat, and cover with an appropriate amount of quartz sand On the top, put into a tubular heating furnace, pass in oxygen and water vapor, gradually heat to 1100°C, and heat at constant temperature for 15 minutes. A 100mL volumetric flask is placed at the lower end of the condenser tube to receive the condensate, and it is controlled within 85mL. After the combustion and hydrolysis are completed, add 3 drops of bromocresol green indicator to the condensate, and neutralize with sodium hydroxide solution until the indicator turns blue. Add ionic strength buffer solution, dilute with water to a constant volume, and leave for half an hour. Using the fluoride ion selective electrode as the indicator electrode a...
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