Octreotide injection
a technology of octreotide and injection, which is applied in the direction of peptide/protein ingredients, cyclic peptide ingredients, non-active ingredients of pharmaceuticals, etc., can solve the problems of poor bioavailability of peptide drugs after oral or parenteral administration, and achieve the effect of improving the bioavailability of peptide drugs
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example 1
[0055]Sterile solution of octreotide acetate according to one embodiment of the present invention is described below.
TABLE 1Sterile solution of the present inventionSr.No.Ingredientsmg / ml1Octreotide acetate equivalent to2.5octreotide base2Lactic acid3.43Mannitol22.54Phenol5.05Sodium bicarbonateq.s. to pH 4.2 ± 0.36Water for injectionq.s to 1 ml
[0056]Procedure: Specified volume of water for injection was collected in suitable container at a temperature of 20° C. to 25° C. To this octreotide acetate was added under stirring to form a clear solution. Specified quantity of lactic acid was dissolved in above solution under stirring until the clear solution was obtained. Specified quantity of mannitol was dissolved in the above solution under stirring until the clear solution was obtained. Separately phenol was dissolved in the specified quantity of water and added to the above bulk solution. Further, the pH of the solution was adjusted to about 4.20±0.30 with sufficient quantity of sodiu...
example 2
[0060]The aqueous solution of octreotide acetate having concentration equivalent to 2.5 mg / ml of octreotide base filled in a pen injection device according to example 1 of the present invention, referred to herein as test product A, was subjected to in-vivo plasma pharmacokinetic study in healthy human volunteers, whereby a given dose of octreotide acetate solution (equivalent to 100 μg octreotide base) was delivered sub-cutaneously through the multiple dose pen injection device to the human volunteer and plasma pharmacokinetic profile of octreotide was studied. The bioavailability i.e. AUC0-∞, AUC0-t, Cmax, Tmax, and other pharmacokinetic parameters were determined. The study was a randomized, open label, two treatment, two period, two sequence, single dose, cross-over study, under fasting conditions and involving twelve healthy adult human volunteers, with a washout period of 7 days between dosages. The marketed product Sandostatin™ 1.0 mg / ml solution in multi-dose vial was taken ...
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