Biodegradable linear random copolyester and its preparation method and uses
A technology of copolyester and aromatic copolyester, applied in the direction of polyester coating, single-component polyester rayon, coating, etc., can solve the problems of many side reactions, serious side reactions, poor stability of polyester products, etc.
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Embodiment A1-6
[0098] Example A1-6 Preparation of rare earth catalyst Cat2
Embodiment A1
[0099] Example A1 Preparation of anhydrous lanthanum chloride (LaCl3) (document J Inorg Nucl Chem 1962, 34, 387)
[0100] Dissolve 10g of La2O3 in excess hydrochloric acid, heat (temperature ≥100℃) to concentrate the solution, add a metered amount of NH4C1 (molar ratio to La2O3 is 3 / 1), carefully heat (temperature ≥100℃) to steam off the excess acid to obtain LaCl3·nH2O+NH4C1 solid, grind the solid and add it to the quartz sublimation tube, vacuumize to <5mmHg; slowly heat up to 400℃ in the tube furnace, vacuum for 1hr; cool to room temperature under vacuum, and sublimate Fill the tube with argon gas, remove the sublimation tube, and move it into another sealed tube for use under the protection of argon gas.
Embodiment A2
[0101] Example A2 Preparation of lanthanum acetylacetonate La(acac)3 (Document Polymer 2001, 42, 7511-7516)
[0102] In a 250ml three-necked flask, dissolve LaCl3·7H2O (3.47g, 9.37mmol) in 50ml of water to form a solution s1. Add s1 dropwise to acetylacetone (5.63g, 56.2mmol) in 50ml aqueous solution s2 at room temperature Under stirring, adjust the pH to 7 by adding 2NKOH solution. The reaction mixture contained La(acac)3 precipitate, stirred, filtered, and dried under vacuum at 60°C to obtain about 4g of La(acac)3.
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