2788results about How to "Smooth response" patented technology

The invention discloses an application of load non- metallocene catalyst in the slurry process for vinyl polymerying, the load non- metallocene catalyst and catalyst promoter forming the catalytic system, the alkene polymerization comprising: vinyl homopolymerization, combined polymerization of vinyl with propylene, butylenes, hexane, octane or norbornene; the catalyst carrier being chosen from: inorganic oxide of metallic oxide from IIA, IIIA, IVA, and IVB groups, or oxided mixture and mixing oxide; the catalyst promoter being chosen from: methylaluoxane, ethylaluoxane, isobutylaluoxane, trimethylaluminum,triethylaluminum,triisobutylaluminum,methylaluoxane-trimethylaluminum or methylaluoxane-triethylaluminum; the mole proportion between the catalyst promoter and catalyst being Al/Ti= 1:1-500. The inventioin is characterized by the less methylaluoxane consumption, stable reaction, easy-to-control polymerization temperature and non still-sticking phenomenon. The produced polyolefine possesses perfect granual shape, and the maximum polymer clamp density can reach 0.385 g/ml.

The invention discloses a biodegradable linear random copolyester, its preparation method and uses, wherein the copolyester has a structural unit of (1), wherein m is an integer of 2-10, n is an integer of 0-8, p is an integer of 2-10, m, n, p are identical or different, x is an integer of 1-10, y is an integer of 1-10, the average molecular weight Mw of the copolyester is 100,000-600,000g/mol, its molecular weight distribution is 1.2-3, which is measured through GPC method. The copolyester can be widely applied into section bar, film, fabric and coating.

The invention provides a preparation method of an epoxy-modified insulated thermal-conductive high-temperature resistant organosilicon coating, comprising the following steps: preparing raw materials; synthesizing an organosilicon pre-polymer; synthesizing an epoxy-modified organosilicon resin; and preparing the epoxy-modified insulated thermal-conductive high-temperature resistant organosilicon coating. The invention also provided the epoxy-modified insulated thermal-conductive high-temperature resistant organosilicon coating prepared by the method. The coating is composed by the epoxy modified organosilicon resin, fillers, a coupling agent and solvents. The coating prepared by the method in the invention takes account of insulation, thermal-conductivity, and high-temperature resistance at the same time, has coating adhesion of first level, hardness of 5H, a breakdown voltage of 1800V/0.5mA, 2 seconds, a heat transfer coefficient of larger than 100W/(m<2>.K), and no obviously changed coating at a temperature of 250 DEG C for 24 hours, therefore the coating can be widely used in various industrial equipment and household appliances.

The invention discloses a production method for manganese sulfate by using low-grade manganese ores. According to the method, manganese sulfate with high purity can be produced by using waste low-grade manganese ores with manganese content of 10% to 20%, manganese tailing or manganese-containing solid waste residue. The method comprises the steps of preparation of raw materials, a slaking reaction, a leaching reaction, neutralization and purification of leachate, etc. According to the invention, production of manganese sulfate is not restricted by the grade of manganese ores, and low-grade manganese oxide ores with a grade greater than 10%, manganese tailing or manganese-containing solid waste residue can be fully utilized; produced manganese sulfate has high yield and high purity and is a very important industrial fundamental product; almost no external heat supply is needed, low energy consumption is achieved, production cost is low, it does not need to turn over and mix materials in the process of the reactions, the reactions are smooth, no toxic gas is generated, and no environmental pollution is produced; discharge of three wastes (waste gas, waste water and industrial residue) reaches national discharge standards for environmental protection, and there is no dust pollution in a workshop.

The present invention relates to a method for preparing chitin and chitosan oligosac charide. The method comprises the steps that usual raw materials such as the crust of shrimp and crab, the insect crust or the fungal mycelia, etc. are micronized through the dry process or wet process; the carapace material of the obtained fine powder raw material is decalcified with the chemical process, and then is defatted and deproteinized with the method of micro-organism compound enzyme coarse enzyme liquid co-enzymolysis, and the insect and fungus fine powder thereof is directly defatted and deproteinized; a whole cell immobilizing bioreactor of a chitin deacetylase high-yield producing strain is prepared, to perform the circulatory deacetylation to the chitin and then obtain chitosan with corresponding degree of deacetylatoion; obligate anaerobic acid-producing bacterium and high-yield producing chitosan bacterium are utilized, the chitosan is submerged and fermented in the liquid, to obtain chitosan oligosaccharide with high water solubility. The present invention has the advantages that the method is helpful to fully utilize the resources, and makes the waste to the worth, at the same time, the default of the manufacturing process of the chemical process can be avoided, the production efficiency is improved, the energy is saved, the consumption is reduced, the byproduct with corresponding high value added can be produced, the comprehensive economic benefits of the relative secondary industry are obviously improved, the industrial development is promoted, and the multi-win effect is attained.

A transducer (14) for producing a force which excites an acoustic radiator, e.g. a panel (12) to produce an acoustic output. The transducer (14) has an intended operative frequency range and comprises a resonant element which has a distribution of modes and which is modal in the operative frequency range. Parameters of the transducer (14) may be adjusted to improve the modality of the resonant element. A loudspeaker (10) or a microphone may incorporate the transducer.

A closed-loop permanent magnet motor control method and system optimally partitions torque and flux-weakening currents to produce a desired torque without exceeding the capability of the DC source. A maximum limit for allowable torque current and a minimum threshold for the maximum torque current are determined, and the flux current is varied based at least in part on whether the maximum torque current limit is above or below the minimum threshold while operating in a flux-weakening region to compensate for the variability of the DC source voltage.

The invention discloses a homogenous low-heat-conductivity inorganic heat insulation board and a preparation method thereof. The homogenous low-heat-conductivity inorganic heat insulation board is prepared from the reaction of an inorganic material, filler and polyurethane hard foam and prepared from the following raw materials in parts by weight: 31 to 85 parts of the inorganic material, 0 to 20parts of the filler, and 15 to 49 parts of the polyurethane hard foam. The heat conduction coefficient of the prepared insulation board is less than 40mW/(m.K), the integral density is 35 to 500 kg/m<3>, and the thermal insulation and heat preservation performance is good. The compressive strength is greater than or equal to 0.1MPa, the tensile strength is greater than or equal to 0.1MPa, the mechanical strength is high, and the durability is good. The oxygen index is greater than or equal to 30 percent, the combustion growth rate index is less than or equal to 120W/s, the total heat release amount in 600s is less than or equal to 7.5MJ, and the homogeneous low-heat-conductivity inorganic insulation board is difficult to combust and high in fireproof grade. The preparation process is simple and suitable for the industrialized production.

A novel aqua regia system ITO etching solution is characterized in that the etching solution comprises hydrochloric acid, nitric acid, pure water and additives, wherein the additives comprise a nitrate compound, a chlorine-based compound and a surfactant. A preparation method of the etching solution comprises the following steps: 1, adding a highly-acidic ion exchange resin to hydrochloric acid and nitric acid respectively, stirring to mix, filtering out the highly-acidic ion exchange resin, and controlling or removing impurity ions in the hydrochloric acid and the nitric acid; 2, weighing the hydrochloric acid, the nitric acid, the chlorine-based compound, the nitro-compound, the surfactant and the pure water according to a ratio; 3, dissolving the chlorine-based compound, the nitro-compound and the surfactant in water, and uniformly mixing the resulting solution with the nitric acid and the hydrochloric acid; and 4, letting the mixture obtained in step 3 in a filterer, and filtering to obtain the ITO etching solution. The etching solution has the advantages of stability, moderate etching efficiency, and good etching efficiency.

The invention relates to a polymer mobility control agent suitable for an ultrahigh-salinity oil deposit and a preparation method thereof, and the polymer mobility control agent is mainly used for solving the problem that a polymer can not meet the requirement for tertiary oil recovery due to poor temperature resistant property, salt resistant property and shearing resistant property in the prior art. In order to better solve the problem, the technical scheme adopted by the invention is as follows: the control agent for an amphoteric hydrophobic associated polymer comprises the following components in parts by weight of the amphoteric hydrophobic associated polymer: 5-99.9 parts of nonionic water-soluble monomers, 0-50 parts of anionic monomers or/and cationic monomers, 0.1-10 parts of hydrophobic monomers with surface activity, 0.1-5 parts of inorganic substances and 1-20 parts of surface active agents. The preparation method disclosed by the invention can be used for the industrial production of the polymer mobility control agent suitable for the ultrahigh-salinity oil deposit.

The invention discloses a catalyst for synthesizing 5-hydroxymethylfurfural by hexose dehydration and a method for synthesizing the 5-hydroxymethylfurfural by using the catalyst. The catalyst consists of iron halide and ammonium halide, and the molar ratio of the iron halide to the ammonium halide is 0.1 to 10. The synthesizing method comprises the following steps: dissolving a reaction substrate into a solvent, adding the catalyst consisting of the iron halide and the ammonium halide into the solution, reacting the solution for 0.5 hour at the temperature of between 0 and 200 DEG C, distilling and condensing the solution, performing extraction, distilling the concentrate under reduced pressure, drying the distillate and collecting a product. The catalyst of the invention overcomes the defects that the catalyst in the prior art has large toxicity and the catalytic reaction needs a large amount of organic solvent and additive. The catalyst totally shows the characteristic of a homogeneous catalyst in the reaction process, and has high catalytic activity and high selectivity; and the using amount of the catalyst can be optimized to trace so as to facilitate the separation and purification of the reaction product. The catalyst has the advantages of simple reaction system, environment friendliness, low toxicity, low production cost and easy post treatment.

The invention relates to a preparation technique of a medicine alogliptin benzoate for treating Type 2 diabetes. The technique comprises the following steps: reacting the raw material 6-chloro-3-methyluracil with 2-cyanobenzyl bromide to prepare 2-(6-chloro-3-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidyl-ylmethyl)-benzonitrile, and carrying out substitution reaction with (R)-3-Boc-aminopiperidine; after the reaction finishes, removing Boc to obtain alogliptin; and finally, salifying with benzoic acid to obtain the alogliptin benzoate. The invention is characterized in that in the substitution reaction, the acid binding agent potassium carbonate is added; and after the reaction finishes, filtration is carried out, and p-toluenesulfonic acid is added into the filtrate to remove the Boc. The preparation technique provided by the invention has the advantages of simple procedure, higher product yield and higher product purity.

The invention discloses a treatment process of waste water polluted by the pesticide of Dursban, and the process includes the procedures of acid eduction, complexation and extraction, Fenton oxidation and catalytic oxidation. The invention is characterized in that Dursban waste water and herbicide Pendimethalin waste water are comprehensively treated, thereby achieving the proposal of waste controlled by the waste, decreasing the load of organic pollutant being hard to be graded in the waste water, improving the biological degradability of the waste water, removing the pollutant from the waste water, and increasing the biochemical performance of the waste water. Besides, the invention has the advantages of safe and advanced technique, clean operation and low waste water treatment cost.

The present invention relates to the preparation and use of alkylphenol ethoxylate (methyl) acrylic ester. The preparation is preferably a ester exchange reaction process including azeotropic dewatering of the mixture of alkylphenol ethoxylate and acrylic ester or methyl acrylic ester in the presence of azeotropic solvent and polymerization inhibitor, ester exchange reaction in the presence of catalyst, separating and recovering azeotropic solvent and acrylic ester or methyl acrylic ester to obtain alkylphenol ethoxylate (methyl) acrylic ester. The technological process is simple and has no polymerization of the material in the reactor and separating tower, good product appearance and alkylphenol ethoxylate converting rate up to 80-95 %.

The present invention relates to chemical reaction process of oxidizing alcohol with oxygen to prepare aldehyde or ketone, and is especially an alcohol oxidizing process with 2, 2, 6, 6-tetramethyl piperidine nitroxide free radical as catalyst. In organic solvent, and in the presence of catalyst comprising TEMPO, sodium nitrite and transition metal salt, alcohol is oxidized to produce aldehyde or ketone. The process has the alcohol, TEMPO, sodium nitrite and transition metal salt in the weight ratio of 100 to 1-5 to 1-10 to 1-10, oxygen pressure of 0.1-0.8 MPa, reaction temperature of 0-80 deg.c and reaction time of 1-24 hr. The present invention has the advantages of mild reaction condition, easy control, low cost, high safety and environment friendship.

The invention belongs to the technical field of chemical processes and equipment, and relates to a device for preparing chlorinated polyvinyl chloride by a gas-solid phase method and a method thereof. The chlorinated polyvinyl chloride is prepared from polyvinyl chloride (PVC) and chlorine gas serving as raw materials in a dry state. The device comprises a riser reactor, a turbulent fluidized bed reactor, an upper connecting pipe and a lower connecting pipe, wherein the synthesis of the chlorinated polyvinyl chloride is performed in the riser reactor and the turbulent fluidized bed reactor; a chain initiation process is realized and chain transfer is finished by activating the chlorine gas with ultraviolet light, so that the whole process is decoupled into a quick process and a slow process, the chlorination of the materials is uniform, bonding and discoloration can be effectively prevented, the energy consumption is reduced and the operation is simplified; the device has the advantages of compact structure, high practicability and obvious improvement on the efficiency; hydrogen chloride separated from reaction tail gas can be recycled; and the whole process has no waste discharge.

A new circuit for producing simulated electrostatic discharges (ESD) based on the Human Body Model (HBM) is disclosed for testing integrated circuits. HBM ESD test systems provide stress pulses defined by industry standards. The pulses produced by prior art have small imperfections or anomalies. These anomalies can cause incorrect testing to certain devices. The improved ESD HBM test system herein disclosed provides pulses meeting the requirements of industry standards while reducing several anomalies to negligible levels.

The invention relates to a profile controlling and flooding composition for high-temperature oil reservoirs with high salinity and an application of the composition in tertiary oil recovery of the high-temperature oil reservoirs with high salinity, and mainly aims at solving the problems of poor heat resistance and salt tolerance and low oil displacement efficiency of an oil displacement agent under the conditions of high temperature and high salinity in the prior art. The problems are well solved by virtue of the following technical scheme: the profile controlling and flooding composition for high-temperature oil reservoirs with high salinity is prepared from the following components in percentage by weight: (1) 0.01-3.0% of heat-resistant and salt-tolerant polyacrylamide microspheres, (2) 0.01-5.0% of anionic-nonionic surfactant and (3) 92.0-99.98% of injected water; and the profile controlling and flooding composition can be applied to field applications for increasing the recovery rate such as depth profile controlling, water plugging and oil displacement for tertiary oil recovery of the high-temperature oil reservoirs with high salinity.

A process for preparing a pyridone derivative (4), which comprises reacting the compound (1) with a hypochlorite or a hypobromite or with lead tetraacetate to give the compound (2), and reacting the compound (2) with the compound (3). Said process is preferably especially from the standpoint of safety. wherein R1 is hydrogen, alkyl, substituted alkyl, etc.; Y1 is hydrogen, alky, substituted alky, etc.; Y2 and Y3 are indenpently hydrogen, halogen, etc.; and L is alkyl, substituted alkyl, etc.

The invention relates to low-moisture low-variable serial saturation tower thermal CO transformation technology, which comprises the following steps: after processing gas-liquid separation, heat exchange and detoxification to crude gas, feeding the crude gas into a pre-transformation furnace to process initial transformation reaction; controlling the mol ratio of crude gas water/dry gas which enters the pre-transformation furnace within 0.19-0.23, and controlling the temperature thereof within 200-220 degrees centigrade; feeding pre-transformed mixing gas from a crude pre-heater into a saturation tower and contact with technical circular water of a hot water tower reversely so as to transmit heat and quality; increasing humidity and temperature of the pre-transformed mixing gas, feeding into the pre-transformed mixing gas into an isothermal transformation furnace so as to process depth transformation; exchanging gas and heat of the isothermal exchange gas of the isothermal transformation furnace so as to feed into the hot water tower to transmit the heat and quality; and recycling low-order heat energy. Compared with the prior art, the isothermal transformation furnace substitutes at least two grades of heat isolating transformation furnaces; the number of transformation furnaces is reduced; equipment investment and catalyst cost are saved; in addition, a transformation procedure is short, resistance is small, energy consumption is low and operation is stable.