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Method for preparing liquid crystal vertical oriented membrane

A vertical alignment and liquid crystal technology, applied in optics, instruments, nonlinear optics, etc., can solve the few problems such as preparing liquid crystal vertical alignment film, and achieve the effect of simplified process and simple process

Inactive Publication Date: 2009-04-08
CHANGCHUN INST OF OPTICS FINE MECHANICS & PHYSICS CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, the photo-controlled alignment method is often used to prepare parallel alignment films of liquid crystal molecules, and is rarely used to prepare vertical alignment films of liquid crystals.

Method used

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  • Method for preparing liquid crystal vertical oriented membrane
  • Method for preparing liquid crystal vertical oriented membrane
  • Method for preparing liquid crystal vertical oriented membrane

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Embodiment Construction

[0027] 1) Synthesis of hexafluorobisphenol A dicinnamate monomer

[0028] Take 3.31 g of hexafluoro-substituted bisphenol A (Aldrich Co., USA) and dissolve it in 40 mL of anhydrous tetrahydrofuran (Tianjin Tiantai Chemical Company, imported sub-packaging), and place it in a 100 mL three-necked bottle. Then take 2.76 mL of triethylamine (Shenyang Dongxing Chemical Factory) and add it directly into the three-necked bottle.

[0029] Take 4.1 g of cinnamoyl chloride (Aldrich Co., USA) and dissolve it in 10 mL of anhydrous tetrahydrofuran, and then place it in a 50 mL dropping funnel.

[0030] Under ice water cooling, the solution of cinnamoyl chloride was slowly added dropwise into the three-necked flask, and at the same time, the automatic stirrer was turned on to stir, and a large amount of white insoluble matter was formed. After the dropwise addition was complete, stirring was continued for 30 minutes.

[0031] The insoluble matter was filtered off to obtain a colorless and ...

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Abstract

This invention is a method of producing the liquid crystal vertical tropism membrane. This invention chooses the monomer with cinnamonic acid structure at both ends of the molecule, and the hexafluorodiphene A dicinnamonic acid ester containing fluoroform radicle. At the normal temperature, dissolve the hexafluorodiphene A dicinnamonic acid ester in the solvent of quadplex hydroxy furan to confect into solution. Smear the solution on the basal board reelingly to form membrane. Shine the monomer membrane material of the hexafluorodiphene A dicinnamonic acid ester with the ultraviolet radiation, and make the both ends of the monomer molecule take place [2+2] cycloaddition reaction, then produce a tropism membrane that can induce the liquid crystal vertical tropism array. This invention avoids heat treatment at high temperature in the confecting process, which consumedly simplified the traditional technics of confecting the liquid crystal vertical tropism membrane. Compared with the traditional method of confecting the liquid crystal vertical tropism membrane, this invention has a simpler technics, and is a new method of confecting the liquid crystal vertical tropism membrane.

Description

technical field [0001] The invention belongs to the technical field of optoelectronic materials, and relates to the preparation of an alignment film of a liquid crystal device, in particular to a method for preparing a vertical alignment film of a liquid crystal. Background technique [0002] Liquid crystal display is favored by people in the field of information display because of its flat panel, easy to carry, low power consumption, no electromagnetic radiation, and no damage to eyesight. However, the shortcomings of narrow viewing angle and slow response speed limit the application of liquid crystal displays. Although the response speed of ferroelectric liquid crystals is much faster than that of nematic liquid crystals, a practical stable alignment method has not been found so far. In twisted nematic liquid crystal display (TN-LCD), super twisted nematic liquid crystal display (STN-LCD), thin film transistor twisted nematic liquid crystal display (TFT-TN-LCD), vertical ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G02F1/1337G02F1/139G02F1/1334
Inventor 宣丽于涛彭增辉刘永刚胡立发
Owner CHANGCHUN INST OF OPTICS FINE MECHANICS & PHYSICS CHINESE ACAD OF SCI
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