Carbonate reference material
A standard substance and carbonate technology, which is applied in the direction of measuring devices, instruments, and material analysis through optical means, can solve problems such as unfavorable development of oil and gas geochemical exploration technology, difficult measurement result monitoring, and difficult measurement results
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Embodiment 1
[0030]Select the Luoji block in the Hefei Basin to collect near-surface soil samples with a sampling volume of 100kg and a sampling depth of 2.0-2.5m. After the samples are coarsely crushed, ground, and mixed, a soil sample that meets the requirements of the carbonate standard sample test is prepared. The prepared samples were tested by variance analysis method (F test method) and average value consistency test method (T test method), which proved that their uniformity and stability were good.
[0031] Carbonate samples were analyzed in accordance with the relevant provisions of "Determination of Carbonate in Oil and Gas Prospecting Soil (Rock) Samples - Volumetric Method (DS / T02.11-2000)". According to the analysis procedure of the present invention, take sample 0.2g, add 15.00ml concentration to the sample and be the hydrochloric acid of 0.1mol / L, back drip with the sodium hydroxide solution of same concentration. The amount and concentration of hydrochloric acid and sodium...
Embodiment 2
[0033] The Luoji block in the Hefei Basin and the Xiakou block in the Jiyang Sag were selected to collect 50 kg of near-surface soil samples each, with a total sampling volume of 100 kg and a sampling depth of 2.0-2.5 m. The samples are crushed, ground, mixed and other processes to prepare soil samples that meet the requirements of the carbonate standard sample test. The prepared samples were tested by variance analysis method (F test method) and average value consistency test method (T test method), which proved that their uniformity and stability were good.
[0034] Carbonate samples were analyzed in accordance with the relevant provisions of "Determination of Carbonate in Oil and Gas Prospecting Soil (Rock) Samples - Volumetric Method (DS / T02.11-2000)". According to the analysis procedure of the present invention, take sample 0.2g, add 15ml concentration to sample and be the hydrochloric acid of 0.1mol / L, back drip with the sodium hydroxide solution of same concentration. ...
Embodiment 3
[0036] The Xiakou Block of Jiyang Depression was selected to collect near-surface soil samples with a sampling volume of 100kg and a sampling depth of 1.5-2.0m. The samples are crushed, ground, mixed and other processes to prepare soil samples that meet the requirements of the carbonate standard sample test. The prepared samples were tested by variance analysis method (F test method) and average value consistency test method (T test method), which proved that their uniformity and stability were good.
[0037] Carbonate samples were analyzed in accordance with the relevant provisions of "Determination of Carbonate in Oil and Gas Prospecting Soil (Rock) Samples - Volumetric Method (DS / T02.11-2000)". According to the analysis program of the present invention, 0.1 g of the sample is weighed. Add 15ml of hydrochloric acid with a concentration of 0.1mol / L to the sample, and back-titrate with a sodium hydroxide solution of the same concentration. The amount and concentration of hyd...
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