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Chinese medicinal composition and preparation method and detection method thereof

A detection method and composition technology, applied in the direction of drug combination, pharmaceutical formulation, measuring device, etc.

Active Publication Date: 2011-05-18
INNER MONGOLIA TIANQI HAN&MONGOLIA PHARMA CO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Looking at the above varieties, their functions and indications include warming kidney yang, nourishing kidney yin, tonifying kidney essence, nourishing qi and blood, clearing heart and liver fire, and adapting to kidney yang deficiency, kidney yin deficiency, yin deficiency and hyperactivity of yang, deficiency of qi and blood or liver Kidney yin deficiency, heart and liver fire, etc., but multiple functions are single

Method used

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  • Chinese medicinal composition and preparation method and detection method thereof
  • Chinese medicinal composition and preparation method and detection method thereof
  • Chinese medicinal composition and preparation method and detection method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0275] Polygonum multiflorum 600g Epimedium 400g Cuscuta 600g

[0276] Polygonum cuspidatum 400g White peony root 400g Chuanxiong 400g

[0277] Excipients: lactose 560g magnesium stearate 5g micronized silica gel 2g aspartame 9g;

[0278] Preparation method: decoct the above six flavors, epimedium, dodder, and white peony with water three times, each time for 1.5 hours, and the amount of water added is 14 times the amount of medicinal materials; combine the decoctions, concentrate to 50 °C, and the relative density is 1.04-1.05, add Ethanol makes the alcohol content of the medicinal solution reach 50%, refrigerate the liquid at 5-10°C, filter, and the supernatant of the alcohol precipitation is ready for use; prepare Polygonum multiflorum, Polygonum cuspidatum, and Ligusticum chuanxiong with 60% ethanol for reflux extraction twice, adding ethanol 6 times each time Double the amount, reflux for 2 hours, combine the alcohol extract, filter to obtain the alcohol extract; take th...

Embodiment 2

[0280] Polygonum multiflorum 650g Epimedium 350g Cuscuta 650g

[0281] Polygonum cuspidatum 350g, white peony root 550g, Chuanxiong 350g;

[0282] Excipients: lactose 660g magnesium stearate 9g micronized silica gel 4g aspartame 12g;

[0283] Preparation method: decoct the above six flavors, epimedium, dodder, and white peony root with water three times, each time for 2 hours, and the amount of water added is 15 times the amount of medicinal materials; combine the decoction, concentrate to 55°C, and the relative density is 1.04-1.05, add Ethanol makes the alcohol content of the medicinal liquid reach 55%, refrigerate the liquid at 5-10°C, filter, and the supernatant of the alcohol precipitation is ready for use; prepare Polygonum multiflorum, Polygonum cuspidatum, and Ligusticum chuanxiong with 66% ethanol for reflux extraction 3 times, each time adding ethanol 6 Double the amount, reflux for 2 hours, combine the alcohol extract, filter to obtain the alcohol extract; take the...

Embodiment 3

[0285] Polygonum multiflorum 550g Epimedium 580g Cuscuta 500g

[0286] Polygonum cuspidatum 460g, white peony root 360g, chuanxiong 460g;

[0287] Preparation method: decoct the above six flavors, epimedium, dodder, and white peony root with water three times, each time for 2 hours, and the amount of water added is 15 times the amount of medicinal materials; combine the decoction, concentrate to 55°C, and the relative density is 1.04-1.05, add Ethanol makes the alcohol content of the medicinal liquid reach 55%, refrigerate the liquid at 5-10°C, filter, and the supernatant of the alcohol precipitation is ready for use; prepare Polygonum multiflorum, Polygonum cuspidatum, and Ligusticum chuanxiong with 66% ethanol for reflux extraction 3 times, each time adding ethanol 6 Double the amount, reflux for 2 hours, combine the alcohol extract, filter to obtain the alcohol extract; take the alcohol extract and the above alcohol precipitation supernatant and combine, recover the ethanol...

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Abstract

The invention discloses a Chinese medicine composite for curing menopause syndrome, a preparation method and quality control method thereof. The medicine comprises the following raw materials: prepared fleeceflower root, epimedium, dodder, bush knotweed root, root of herbaceous peony and szechuan lovage rhizome, and the preparation method is as follows: the epimedium, the dodder and the root of herbaceous peony are boiled in water and ethanol is added for alcohol sedimentation; 50-70 percent of ethanol reflux is used for extracting the prepared fleeceflower root, the bush knotweed root and the szechuan lovage rhizome; alcohol extract is selected to combine with the alcohol sedimentation supernatant, pressure is reduced and the product is dried, and lactose, magnesium stearate, aerosil andaspartame are added for dry pressing and pelletization. The invention adopts high-performance liquid chromatography to test the content of 2, 3, 5, 4-tetrahydroxy-stilbene-2-O-beta-D-glucoside. The Chinese medicine composite has good efficacy of curing menopause syndrome.

Description

technical field [0001] The invention relates to a traditional Chinese medicine composition, a preparation method and a detection method thereof, in particular to a traditional Chinese medicine composition for treating climacteric syndrome, a preparation method and a detection method thereof. Background technique [0002] Menopausal syndrome refers to the symptoms of autonomic nervous system dysfunction caused by the decline of ovarian function and low estrogen level in women before and after menopause. Traditional Chinese medicine believes that it is caused by deficiency of kidney qi and imbalance of yin and yang. According to relevant domestic and foreign statistical reports, 90% of women aged 45-50 have different clinical manifestations. With the advent of an aging society, women with menopausal syndrome are increasing day by day. According to statistics, in 2000, there were about 120 million women over 50 years old in my country, and it will reach about 280 million by 2...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/71A61K9/16A61P15/12G01N30/02G01N30/90
Inventor 廖军鲜
Owner INNER MONGOLIA TIANQI HAN&MONGOLIA PHARMA CO