Imidazolinum salts with low melting points, method for their manufacture and their use as lubricant
An imidazolinium salt and imidazolinium technology are applied in the field of novel low-melting imidazolinium salts and their preparation, and can solve problems such as dangerous discharge
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[0127] In the examples given below, the present invention is described by way of example, and the present invention is not limited to the embodiments specifically illustrated in the examples, and its scope of applicability is determined by the specification and claims.
[0128] All percentages are by weight unless otherwise indicated.
[0129] General preparation of imidazolinium salts without isolation of intermediates (Formula I)
[0130] Initially, at N 2 Next, 1.75 mol of aminoethylethanolamine (AEEA) and 0.01 mol of 30% sodium methoxide were charged into a four-neck glass flask. At 70°C, add 1 mol of the specific carboxylate within 1.5h. This process is accompanied by a slight exotherm, and the temperature should not exceed 90°C. Amidation takes place within 6 to 10 h. For monitoring, infrared spectra were recorded at 1740 nm. Sufficient alkalinity (>2mgKOH / g) must be ensured. Upon completion of the amidation, the alkalinity was neutralized with 85% phosphoric acid, ...
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Abstract
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