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Strong corrosivity medium phase interface measurement method

A phase interface and flow technology, applied in the direction of displaying the liquid level indicator through pressure measurement, can solve the problems of difficult to ensure effective use for a long time, corrosion, and high cost of the instrument, achieving low cost, simple measurement method, Apply a wide range of effects

Inactive Publication Date: 2009-07-29
ZHONGHAO CHENGUANG RES INST OF CHEMICALINDUSTRY CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] However, in the environment of strong corrosive media, such as hydrofluoric acid, hydrochloric acid and other media environments, if you use general instruments such as magnetic levitation liquid level gauges, differential pressure liquid level gauges, etc. to measure the position of the phase interface, it will soon be Corrosion, it is difficult to ensure long-term effective use; if indirect liquid level gauges such as radar are used for measurement, the cost of the instrument is very high; in addition, if the production process needs to separate multi-phase mixtures at the same time, it is also necessary to be able to measure the multi-phase interface. Instrument or method, therefore, the object of the present invention is to provide a method with low cost, capable of measuring multiple phase interfaces at the same time, and especially suitable for phase interfaces of strong corrosive media

Method used

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  • Strong corrosivity medium phase interface measurement method

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Embodiment 1

[0026] The mensuration of embodiment 1 two-phase interface

[0027] The method of the present invention is used to measure the hydrofluoric acid in the upper phase and the phase interface of Freon in the lower phase.

[0028] Using water as the pressure fluid, open the pressure port on the side wall of the equipment, the upper pressure port is connected with the strong acid of the inorganic mixture in the upper layer, and the lower pressure port is connected with the organic mixture, and the relative height of the upper and lower pressure ports is H; ensure the pressure The liquid flows into the device from the upper and lower pressure ports at a certain flow rate (if the pressure of the pressure liquid is lower than the internal pressure of the equipment, a booster pump is required to pressurize the pressure liquid) into the equipment from the upper and lower pressure ports (it is enough to ensure a slight positive pressure at the pressure port) , in order to ensure and measu...

Embodiment 2 3

[0034] The mensuration of embodiment 2 three-phase interface

[0035] The method of the present invention is used to measure that the upper layer is hydrocyanic acid, the middle layer is difluorochloromethane, and the lower layer is CCl 4 Use the medium that is easy to separate from various materials in the equipment: water is used as the pressure fluid, and a pressure port is opened on the side wall of the equipment. The upper pressure port is connected with hydrocyanic acid, and the middle pressure port is connected with difluoro Chloromethane is connected, and the lower pressure port is connected with CCl 4 The relative height between the upper and middle pressure introduction ports is H1, and the relative height between the middle and lower pressure introduction ports is H2; ensure that the pressure induction fluid flows into the equipment from the upper, middle and lower pressure introduction ports at the same flow rate, and the difference The pressure sensors of the pre...

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Abstract

The invention relates to a phase interface measuring method. The method comprises the following steps: pressure liquid is pressed into a phase to be measured from an upper pressure opening and a lower pressure opening at the same flow, pressure of the pressure openings is measured, and phase interface height h (h=(deltaP-rho1*g*H) / (rho2-rho1) / g) is computed according to pressure difference deltaP between the upper pressure opening and the lower pressure opening, the height H of the upper pressure opening as well as upper phase density rho1 and lower phase density rho2 of two phases in the phase to be measured. In the measuring method, a common instrument can measure the phase interface height of highly corrosive media, which has the advantages of low cost, simple measuring method and wide application; and the measuring method can be used for measuring liquid level, the phase interface height between media with similar density and each phase interface height of a multi-phase mixture besides being especially suitable for measuring the phase interface height of the highly corrosive media.

Description

technical field [0001] The invention relates to a method for measuring a phase interface, in particular to a method for measuring a phase interface of a strong corrosive medium. Background technique [0002] In the chemical reaction, there is inevitably a separation process of two-phase or multi-phase media in the system. To realize the continuous, long-term and normal operation of the chemical process, the height of the phase interface in the equipment can be directly and accurately judged, especially The height of the phase interface is especially important in the presence of strong corrosive media. [0003] However, in the environment of strong corrosive media, such as hydrofluoric acid, hydrochloric acid and other media environments, if you use general instruments such as magnetic levitation liquid level gauges, differential pressure liquid level gauges, etc. to measure the position of the phase interface, it will soon be Corrosion, it is difficult to ensure long-term e...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01F23/14
Inventor 谭梅芳曾本忠许鸿禧张金刚余道腾柏荣
Owner ZHONGHAO CHENGUANG RES INST OF CHEMICALINDUSTRY CO LTD
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