Insecticidal water soluble granule of fipronil and preparation thereof

A fipronil and soluble technology, which is applied in the field of plant protection insecticides and its preparation, can solve the problems of human body and plants being poisonous, affecting the health of operators, and inconvenient transportation, so as to reduce pollution, promote environmental protection, Avoid flammable and explosive effects

Active Publication Date: 2012-12-05
佳木斯兴宇生物技术开发有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

As we all know, emulsifiable concentrate contains a large amount of organic solvents, which are easy to volatilize and catch fire, are poisonous to human body and plants, pollute the environment, and are inconvenient to transport; wettable powders will generate a lot of dust during production and use, pollute the environment, and affect the health of operators

Method used

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  • Insecticidal water soluble granule of fipronil and preparation thereof
  • Insecticidal water soluble granule of fipronil and preparation thereof
  • Insecticidal water soluble granule of fipronil and preparation thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Prepare the insecticidal soluble granule containing fipronil of the present invention as follows:

[0026] ①Mix 0.5% fipronil original drug, 1% polyvinyl alcohol, and 4% sodium dodecylbenzenesulfonate in 55°C water, at 420 kg / cm 2 Stir and homogenize under high pressure;

[0027] ②Spray-dry the above-mentioned liquid mixture after homogenization to make a compound parent drug;

[0028] ③ After thermally dissolving 3% nonylphenol polyoxyethylene ether, mix with 3% dispersant NNO, 1% sodium benzoate, 46% sodium bicarbonate, 41.5% anhydrous citric acid and compound parent drug at 45 Heat mixing at ℃ temperature, and then at 4 kg / cm 2 Stir and knead evenly under pressure to obtain a dough;

[0029] ④ Put the bolus at 6 kg / cm 2 Extruded into columnar particles under pressure;

[0030] ⑤ Vacuum-dry the columnar particles at 70°C for 1 hour and then sieve. The sieved products are tested and packaged; the products that cannot pass the sieve are tested and packaged after re...

Embodiment 2

[0034] Prepare the insecticidal soluble granule containing fipronil of the present invention as follows:

[0035] ①Mix 10% fipronil original drug, 1.2% β-cyclodextrin, and 4% fatty amide N-methylsulfonate in 50°C water, at 430 kg / cm 2 Stir and homogenize under high pressure;

[0036] ②Spray-dry the above-mentioned liquid mixture after homogenization to make a compound parent drug;

[0037] ③After dissolving 6% biphenol polyoxyethylene ether and 2% benzylphenol polyoxyethylene ether, mix with 0.8% sodium lignosulfonate, 1% borax, 42% sodium bicarbonate, 33% Anhydrous sodium sulfate and compound parent drug are mixed hot at 45°C, and then heated at 5 kg / cm 2 Stir and knead evenly under pressure to obtain a dough;

[0038] ④ Put the bolus at 8 kg / cm 2 Extruded into columnar particles under pressure;

[0039] ⑤ Vacuum-dry the columnar particles at 70°C for 1 hour and then sieve. The sieved products are tested and packaged; the products that cannot pass the sieve are tested an...

Embodiment 3

[0043] Prepare the insecticidal soluble granule containing fipronil of the present invention as follows:

[0044] ①Mix 30% fipronil original drug, 1% methylcellulose and 4% sodium dodecyl naphthalene sulfonate in 60°C water, 2 Stir and homogenize under high pressure;

[0045] ②Spray-dry the above-mentioned liquid mixture after homogenization to make a compound parent drug;

[0046] ③After dissolving 9% benzyl alkylphenol polyoxyethylene ether, 2% sorbitol fatty acid ester and its ethylene oxide adduct, mix with 3% pull-off powder BX, 1% borax, 20% of maltose, 30% of anhydrous citric acid and compound parent drug are mixed hot at a temperature of 50°C, and then mixed at a temperature of 6 kg / cm 2 Stir and knead evenly under pressure to obtain a dough;

[0047] ④ Put the bolus at 10 kg / cm 2 Extruded into columnar particles under pressure;

[0048] ⑤ Vacuum-dry the columnar particles at 70°C for 1 hour and then sieve. The sieved products are tested and packaged; the products...

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PUM

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Abstract

The invention provides a water soluble granule of fipronil. It is made from (by wt%) fipronil 0.5-50%, emulsifier 1-30%, dispersing agent 1-10%, wetting agent 1-5%, binder 2-4%, stabilizer 1-3% and the rest is filling material. The invention also provides the preparation method of the soluble granule of fipronil, which comprises kneading, extruding, granulating, vacuum drying at 70°C for 1 hour, screening and packaging. The product of the invention has a high insecticidal effect, is of low cost, is safe and convenient to use and is friendly to environment.

Description

technical field [0001] The invention relates to an insecticidal soluble granule containing fipronil and a preparation method thereof, in particular to an insecticide for plant protection containing the insecticidal soluble granule containing fipronil and a preparation method thereof. Background technique [0002] With the continuous improvement of people's living standards, people's awareness of environmental protection, and our government's emphasis on the ecological environment, the domestic and foreign markets are demanding high-efficiency, low-toxicity, low-residue, and non-toxic There is an increasing demand for environmentally friendly bio-pesticides and chemical pesticides that pollute. [0003] There are many types of insecticides for plant protection, and emulsifiable concentrates and wettable powders are generally used. As we all know, emulsifiable concentrate contains a lot of organic solvents, which are easy to volatilize and catch fire, which are poisonous to h...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N25/12A01N43/56A01N25/08A01P7/00
CPCA01N47/02
Inventor 栾贵书王志祥迟云英李海旭刘长春
Owner 佳木斯兴宇生物技术开发有限公司
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