Multi-channel metal palladium or palladium alloy composite membrane hydrogen separator
A multi-channel, metal palladium technology, applied in hydrogen separation, semi-permeable membrane separation, separation methods, etc., can solve problems such as difficult application, leakage at the graphite gasket, and different thermal expansion coefficients
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Embodiment 1
[0036] Take multi-channel Al 2 O 3 The ceramic tube 1 is used as the support of the metal palladium-gold composite membrane 2 and has a length of 250 mm and a diameter of 30 mm. Multi-channel Al 2 O 3 The ceramic tube is composed of 19 holes, the diameter of the holes is 4mm, and the cross-sectional diagram is shown figure 1 . Using conventional electroless plating method, a continuous palladium film is formed on the inner surface of the multi-channel ceramic tube, the cross section 3 at both ends and the outer surface 30mm away from the end. The thickness of the palladium film is about 5μm (the cross section is as figure 2 Shown). A graphite sealing ring 4 is used to connect and seal the multi-channel metal palladium composite membrane with the metal joint 5 at a distance of about 10 mm from the end of the outer surface of the multi-channel metal palladium composite membrane. Then connect the metal joint 5 and the separator shell 6 to form a hydrogen separator, one end of whi...
Embodiment 2
[0054] Take multi-channel Al 2 O 3 The ceramic tube 1 is used as the support of the metal palladium-silver alloy composite membrane 2 and has a length of 250 mm and a diameter of 30 mm. Multi-channel Al 2 O 3 The ceramic tube is composed of 7 holes with a diameter of 6mm. There are grooves 8 on the outer surface 10mm away from both ends. The groove width is 1.5mm and the depth is 0.15mm. Using conventional electroless plating methods, a continuous palladium-silver alloy film is formed on the inner surface of the multi-channel ceramic tube 1, the cross-section 3 at both ends, and the outer surface 30mm from the end (the cross-section is as image 3 Shown). The thickness of the palladium-silver alloy film is about 4.8 μm, and the palladium / silver ratio is 74 / 26. A graphite sealing ring 4 is used to connect and seal the multi-channel metal palladium-silver alloy composite film 2 and the metal joint 5 at the groove 8 on the outer surface of the multi-channel metal palladium silver...
Embodiment 3
[0065] Take multi-channel Al 2 O 3 The ceramic tube 1 is used as the support of the metal palladium composite membrane 2 and has a length of 250 mm and a diameter of 30 mm. Multi-channel Al 2 O 3 The ceramic tube is composed of 19 pores with a diameter of 4mm. There is a slope 9 from the end to 40 mm from the end, the diameter at the end is 30.3 mm, and the diameter at the end 40 mm is 30 mm. Using the conventional electroless plating method, a continuous palladium film is formed on the inner surface of the multi-channel ceramic tube, the cross section 3 at both ends, and the outer surface 30mm away from the end (the cross section is as Figure 4 Shown). The thickness of the palladium film is about 5.2 μm. A graphite sealing ring 4 is used to connect and seal the multi-channel metal palladium composite membrane with the metal joint 5 at a distance about 10 mm from the end of the outer surface of the multi-channel metal palladium composite membrane. Then connect the metal join...
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