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Method and system for controlling automatic growth of zone-melt crystal by adopting diameter process

A technology of automatic growth and zone control, applied in the directions of crystal growth, single crystal growth, chemical instruments and methods, etc., can solve the problems of long artificial crystal pulling time, poor single crystal quality control, and large human factors, so as to reduce artificial The effect of labor intensity, improving consistency quality, reducing errors and losses

Active Publication Date: 2013-02-13
ZHONGHUAN ADVANCED SEMICON MATERIALS CO LTD +1
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AI Technical Summary

Problems solved by technology

At present, the five process sections of the zone melting method basically adopt artificial methods, and the disadvantages of artificial crystal pulling are obvious: 1) When growing large-diameter single crystals, the artificial pulling time is too long, and it is difficult to mass-produce large-diameter single crystals ; 2) In the process of crystal growth, human influence factors are relatively large, and the growth process of the crystal is difficult to control; 3) The quality of the single crystal is poorly controlled, and artificial crystal pulling cannot guarantee that every zone melting single crystal produced has the same quality
[0003] Since there is no research on the automatic growth technology of zone melting crystals in China, it is very necessary to develop a set of zone melting silicon single crystal automatic growth methods and systems

Method used

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  • Method and system for controlling automatic growth of zone-melt crystal by adopting diameter process
  • Method and system for controlling automatic growth of zone-melt crystal by adopting diameter process

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Embodiment Construction

[0027] A specific implementation case of automatic growth of a Φ6" zone melting single crystal is given below to further illustrate how the present invention is realized.

[0028] The specific steps of automatic growth of Φ6" zone melting single crystal are as follows:

[0029] (1) Set the growth interval and set the control parameters

[0030] Set the diameter range, taking this implementation as an example, the set range is 50-60mm, 60-70mm, 70-80mm, 80-90mm, 90-100mm, 100-110mm, 110-120 mm, 120-130mm, 130- 140mm, 140-152mm. Then set the control parameter options of each automatic shoulder single crystal diameter interval based on empirical data, for example: in the corresponding set diameter interval 60-70mm, set V lower The falling speed of the single crystal is 3.6mm / min, the power of the generator is 22kw, the rotation speed of the single crystal is 7.5rpm, the rotation speed of the polycrystal is 0.30rpm, R growth The growth rate of the single crystal is 4.0mm / dia ​​...

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Abstract

The invention relates to a method and system for controlling automatic growth of zone-melt crystal by adopting a diameter process. The method comprises the steps of: setting a growing interval and inputting control parameters; opening a control program when the diameter is more than 50 mm; judging the growing interval by the program according to the detected single crystal diameter and dispatching and calculating the interval parameters; controlling according to the parameters and the calculated value; running the program in the next interval after finishing growing until entering the isometrical growing step; and controlling according to a preset value of a keeping power. The system for controlling automatic growth of zone-melt crystal by adopting the diameter process comprises a PLC controller, a PC, a camera, a generator, a touch screen, an upper-rotating servo motor, a lower-rotating servo motor, a speed-increasing servo motor and a speed-reducing servo motor, a polycrystal rotating motor and a monocrystal rotating motor, a polycrystal descending motor and a monocrystal descending motor, an electromagnetic valve, a flowmeter and a sensor. According to the method and the systemin the invention, the capacity of a zone-melting process for producing large-diameter monocrystals is improved greatly; the artificial error and loss in the zone-melting process are reduced; the working intensity of growing the monocrystals in the zone-melting process is reduced; and the consistency of the monocrystals can be improved effectively.

Description

technical field [0001] The present invention relates to a method and equipment for producing zone-melted silicon single crystals, in particular to a method and system for controlling the automatic growth of zone-melted crystals using the diameter method. Background technique [0002] At present, the production of silicon single crystal by zone melting method mainly uses the method of artificial crystal pulling. The process of growing crystals by zone melting method is mainly composed of preheating and chemical materials, neck and thin neck growth, shoulder shouldering, equal diameter growth, and finishing. At present, the five process sections of the zone melting method basically adopt artificial methods, and the disadvantages of artificial crystal pulling are obvious: 1) When growing large-diameter single crystals, the artificial pulling time is too long, and it is difficult to mass-produce large-diameter single crystals ; 2) During crystal growth, human influence factors ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C30B13/30
Inventor 靳立辉刘嘉王遵义王彦君赵宏波李立伟张雪囡高树良沈浩平
Owner ZHONGHUAN ADVANCED SEMICON MATERIALS CO LTD
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