Preparation method of sweet potato stem-leaf extract
A technology for sweet potato stems and leaves and extracts, which is applied in the field of extracting effective components from sweet potato stems and leaves, and achieves the effects of avoiding waste, saving drying time and achieving continuity
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Embodiment 1
[0030] A preparation method of sweet potato stem and leaf extract, comprising the following steps:
[0031] (1) Freeze-drying and crushing: Freeze the washed fresh sweet potato stems and leaves at -35-45°C, then vacuum-dry them at 25°C-40°C to make the water content 2.5%, and crush them into 60-100 mesh particles;
[0032] (2) Extraction: Add 5 times the weight of the extractant ethanol for extraction, while stirring, extract 5 times, combine the extracts, and concentrate to a density of 1.0g / mL;
[0033] (3) Dry using conventional drying means.
Embodiment 2
[0035] A preparation method of sweet potato stem and leaf extract, comprising the following steps:
[0036] (1) Freeze-drying and crushing: Freeze the washed fresh sweet potato stems and leaves at -35-45°C, then vacuum-dry them at 25°C-40°C to keep the water content below 3%, and crush into 60 ~ 100 mesh particles;
[0037] (2) Extraction: add 10 times the weight of the extractant acetone for extraction, stir at the same time, extract 3 times, combine the extracts, and concentrate to a density of 1.5g / mL;
[0038] (3) Dry using conventional drying means.
Embodiment 3
[0040] A preparation method of sweet potato stem and leaf extract, comprising the following steps:
[0041] (1) Freeze-drying and crushing: Freeze the washed fresh sweet potato stems and leaves at -35-45°C, then vacuum-dry them at 25°C-40°C to keep the water content below 3%, and crush into 20-60 mesh particles;
[0042] (2) Extraction: add 10 times the weight of the extractant ethanol for extraction, and stir at the same time, extract 3 times, combine the extracts, and concentrate to a density of 1.5g / mL;
[0043] (3) Use belt-type vacuum drying for drying. The drying conditions are: first drying zone, temperature 80-95°C, pressure -0.07-0.085 MPa, time 5-8 minutes; second drying zone, temperature 50-80°C , the pressure is -0.05 ~ 0.075 MPa, the time is 50 ~ 100 minutes; the cooling zone, the temperature is 0 ~ 25 ° C, the pressure is -0.07 ~ 0.08 MPa, the time is 15 ~ 25 minutes.
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