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Preparation method of thermoplastic resin/corn husk composite material

A thermoplastic resin and thermoplastic resin film technology, which is applied in the field of thermoplastic resin/corn husk composite material preparation, can solve problems such as research on green composite materials without corn husk coating, and achieves easy operation in process, abundant raw material sources, and wood reduction. the effect of using

Inactive Publication Date: 2015-02-25
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Northwest A&F University’s research on the basic mechanical properties of corn husks shows that corn husks may be used as cushioning materials for making special wood-based panels or packaging, but there is no in-depth research on corn husk green composite materials

Method used

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  • Preparation method of thermoplastic resin/corn husk composite material
  • Preparation method of thermoplastic resin/corn husk composite material
  • Preparation method of thermoplastic resin/corn husk composite material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Preparation of corn husk reinforced polypropylene composites

[0030] (1) Place about 10 grams of polypropylene resin particles between two layers of polyimide film. Then they were placed on a flat vulcanizer, and the parameters of the flat vulcanizer were set as follows: temperature 200° C., pressure 5 MPa, action time 100 seconds. Preheat for 60 seconds first, then heat press for 40 seconds. After hot pressing, it is cooled at room temperature under the action of 2MPa. A polypropylene resin film with a thickness of about 0.1 mm was obtained.

[0031] (2) After cleaning and sorting the corn husks just peeled off from the corn, bake them in an oven at 60°C for 8 hours. Then cut off its head and tail, and flatten it under the action of 0.1MPa.

[0032] (3) Lay the PP film and the corn husks alternately, fix them with a mold and place them between two layers of polyimide films with a thickness of 1 mm and a length and width of 30 cm, which are resistant to high temper...

Embodiment 2

[0034] Preparation of corn husk reinforced polylactic acid resin composites

[0035] (1) Place 10g of polylactic acid resin particles between two layers of polyimide film. Then they were placed on a flat vulcanizer, and the parameters of the flat vulcanizer were set as follows: temperature 200° C., pressure 5 MPa, action time 100 seconds. Preheat for 60 seconds first, then heat press for 40 seconds. After hot pressing, it is cooled at room temperature under the action of 2 MPa. A polylactic acid resin film with a thickness of about 0.1 mm was obtained.

[0036] (2) After cleaning and sorting the corn husks just peeled off from the corn, bake them in an oven at 60°C for 8 hours. Then its head and tail were cut off, and it was flattened under the action of 0.1 gram.

[0037] (3) Lay the PLA film and the corn husk alternately on top of each other, fix them with a mold, and place them between two layers of polyimide films with a thickness of 1 mm and a length and width of 30 c...

Embodiment 3

[0039] Preparation of polybutylene succinate composite material reinforced with corn husk

[0040] (1) 10 g of polybutylene succinate resin particles were placed between two layers of polyimide films. Then they were placed on a flat vulcanizer, and the parameters of the flat vulcanizer were set as follows: temperature 130° C., pressure 5 MPa, action time 100 seconds. Preheat for 60 seconds first, then heat press for 40 seconds. After hot pressing, it is cooled at room temperature under the action of 2 MPa. A polybutylene succinate resin film with a thickness of about 0.1 mm was obtained.

[0041] (2) After cleaning and sorting the corn husks just peeled off from the corn, bake them in an oven at 60°C for 8 hours. Then cut off its head and tail, and flatten it under the action of 0.1MPa.

[0042] (3) Lay the PBS film and the corn bracts in alternate layers, fix them with a mold, and place them between two layers of polyimide films with a thickness of 1 mm and a length and w...

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Abstract

The invention relates to a preparation method of a thermoplastic resin / corn husk composite material. The preparation method comprises the following steps: 1, placing thermoplastic resin particles between two high temperature-resistant films, and carrying out hot pressing and cold pressing to obtain uniform-thickness thermoplastic resin films; 2, drying corn husks, wiping out heads and tails, and planishing to obtain processed corn husks; and 3, alternatively laminating the thermoplastic resin films and the processed corn husks, fixing, carrying out hot pressing, infiltrating the corn husks after the resins are completely melted, and solidifying under conditions that the pressure is 0.5-5MPa and the temperature is normal temperature. The preparation method of the invention has the advantages of simplicity, abundant raw material sources, low cost, and high production efficiency, and is suitable for large-scale industrial production; and the prepared thermoplastic resin / corn husk composite material prepared in the invention has good mechanical performances and a good sound insulation effect, and can be used for processing artificial sheets to reduce the use of timbers.

Description

technical field [0001] The invention belongs to the field of preparation of thermoplastic resin composite materials, in particular to a preparation method of thermoplastic resin / corn husk composite materials. Background technique [0002] Corn husk is a special part of corn stalk. It is a soft unidirectional reinforced composite material wrapped on the corn cob fruit. It is rich in resources, low in price and excellent in performance. Corn husks are rich in cellulose, hemicellulose and lignin (above 75%). Compared with corn stalk extracts and other substances that have a negative impact on mechanical properties, the surface texture is fine and the longitudinal strength (tensile, shear Cut) is high, and the moisture content has little effect on the longitudinal strength. [0003] Corn is one of the main crops in my country. According to the latest statistics, in 2011, the planting area of ​​corn in my country reached 32.3 million hectares, and the yield of corn bracts per he...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B29C70/34B29C70/54
Inventor 许福军赵鹏伟邓惠文顾伟韩昊刘丽佳邱夷平
Owner DONGHUA UNIV