A multi-stage atomized heavy oil catalytic cracking anti-coking nozzle

A heavy oil catalysis and anti-coking technology, which is applied in catalytic cracking, cracking, petroleum industry, etc., can solve the problems of catalyst breakage, steam injection hole wear, high feed oil injection speed, etc., to suppress ejection backflow, destroy oil film accumulation, eliminate The effect of large droplets

Active Publication Date: 2014-10-29
LUOYANG SENDE PETROCHEM ENG
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, in the actual use process, the above-mentioned nozzles have more or less the following problems: first, the atomization effect of the feedstock oil needs to be further improved; Coking phenomenon occurs; the third is that the injection speed of the atomized raw material oil droplets sprayed out by the nozzle is too high, which seriously breaks the catalyst; the fourth is that the atomized steam and the raw material oil interact with each other in the inlet area of ​​the nozzle, and even appear when the fog When the pressure of steam (or raw oil) fluctuates, the raw oil (or atomized steam) cannot be introduced into the nozzle
[0007] Through research, it is found that the shortcomings of 200410010045.3 mainly lie in two aspects: one is that there is still an accumulation of oil film on the inner wall of the local area inside the nozzle; "Sensitive" because the 200410010045.3 steam injection hole is connected with the secondary steam chamber. When the steam pressure and flow fluctuate, or even the raw oil flow fluctuates, it may cause the catalyst to suck back and even cause the steam injection hole to wear

Method used

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  • A multi-stage atomized heavy oil catalytic cracking anti-coking nozzle
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  • A multi-stage atomized heavy oil catalytic cracking anti-coking nozzle

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Effect test

Embodiment 1

[0050] Such as figure 1 , figure 2 , image 3 and combine Figure 7 , a multi-stage atomized heavy oil catalytic cracking anti-coking nozzle, the nozzle includes an inner pipe 5, an outer pipe 3, a nozzle 1, a raw oil inlet 14 and a primary steam inlet 15; the inner pipe 5 and the outer pipe 6 The annular cavity between them constitutes the annular secondary steam chamber 4, and a secondary steam inlet 9 is arranged on the side away from the nozzle; the inner pipe 5 has a constriction section 8, a throat section 7 and a diffusion section 6, and the spray head The front end has a nozzle outlet 19; the feed oil inlet 14 communicates with the manifold chamber 13, and communicates with the frustum-shaped mixing chamber 10 through a plurality of evenly distributed feed oil nozzles 12 at a certain angle to the nozzle axis, so that When the raw oil enters the mixing chamber, it is divided into multiple fine jets. Due to the sudden drop in pressure at the raw oil nozzle 12, the ra...

Embodiment 2

[0064] Such as Figure 4 , Figure 5 , Figure 6 and combine Figure 7 , the main scheme of this embodiment is the same as that of embodiment 1. In this embodiment, the primary steam nozzle adopts the form of connecting pipe 11; and the raw material oil nozzle 12 adopts the form of direct drilling. This embodiment is suitable for the flow of raw material oil less than 5t / h At this time, the overall size of the nozzle is small, and it is difficult to weld the pipe at the inlet end of the mixing chamber 10, but at this time the thickness of the orifice plate at the inlet end of the mixing chamber is not less than 10 mm.

Embodiment 3

[0066] Such as Figure 8 , Figure 9 , Figure 10 and combine Figure 11 , the main scheme of this embodiment is the same as that of embodiment 1, and the difference between this embodiment and embodiment 1 and embodiment 2 in this embodiment is the form of the primary steam nozzle 11 and the raw material oil nozzle 12 in the mixing chamber 10 parts, and the primary steam is Introduced by the primary steam inlet 15, it first enters the primary steam distribution chamber 16, and then enters the mixing chamber 10 through the primary steam nozzle 11. There are one or more primary steam nozzles 11 arranged at the inlet end of the mixing chamber 10, and there are nine in this embodiment. (Such as Figure 9 As shown in the concentric double circle), the primary steam outlet 11 is parallel to the axis of the nozzle, and adopts the form of a connecting pipe.

[0067]After the heated raw oil enters the nozzle from the raw oil inlet 14, it first enters the manifold chamber 13 of the...

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Abstract

The invention belongs to a catalytic cracking device in the field of petroleum refining and provides a multistage atomized heavy oil catalytic cracking anti-coking nozzle. The multistage atomized heavy oil catalytic cracking anti-coking nozzle comprises an inner tube (5), an outer tube (3), a shower nozzle (1), a raw oil inlet (14) and a primary steam inlet (15), the raw oil inlet (14) is communicated with a collecting tube chamber (13) and is communicated with a mixing chamber (10) in a shape of a circular truncated cone through a plurality of evenly-distributed raw oil nozzles (12), and the first stage pulverization of raw oil is obtained when the raw oil enters the mixing chamber. The second stage pulverization is carried out on the raw oil in the mixing chamber through primary steam sprayed in the mixing chamber from a primary steam nozzle (11). The third stage pulverization is carried out on the raw oil in the inner tube after the second stage pulverization. A secondary steam spraying hole I (2-2) enables the raw oil to conduct the fourth stage pulverization. The multistage atomized heavy oil catalytic cracking anti-coking nozzle adopts a multistage atomizing mode to strengthen pulverization effects, therefore, coking of the raw oil on the wall of a riser reactor is avoided.

Description

technical field [0001] The invention belongs to a catalytic cracking device in the field of petroleum refining, and mainly relates to a multi-stage atomization heavy oil catalytic cracking anti-coking nozzle. Background technique [0002] Raw oil feeding atomization nozzle is an important equipment of catalytic cracking unit in the field of petroleum refining. In the tube reactor, it mixes and reacts with the catalyst in the riser reactor. [0003] In recent years, the feed oil atomization nozzles used in catalytic cracking units mainly include throat type LPC type (90209410.6), KH type with supersonic atomizing steam double throat type (89207961.9, 200420066089.3), BWJ type with swirl structure (98233035.9,), UPC-ɑ type with porous steam distributor (00109776.8), and CCK type with secondary atomization structure (99219391.5); foreign similar technologies mainly include S&W The company's target nozzle, the multi-nozzle Optimix nozzle with a built-in porous steam distributo...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10G11/00
Inventor 范怡平吴朝能陈维许煜许栋五
Owner LUOYANG SENDE PETROCHEM ENG
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