Visible-light photocatalytic material and preparation method thereof
A photocatalytic material and visible light technology, applied in the field of photocatalytic materials, can solve the problems of unfavorable large-scale production of organic solvents, limited space for improvement, cumbersome preparation process, etc., achieve good visible light absorption, increase separation, and simple preparation process. Effect
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Embodiment 1
[0015] (1) Preparation of bismuth oxychloride with flake structure: Weigh 0.5g of bismuth nitrate pentahydrate and 0.077g of potassium chloride and mix them in a beaker filled with deionized water, then stir the mixture at room temperature for 30min, and finally transfer to In a 25ml airtight autoclave containing polytetrafluoroethylene lining, the filling volume of the autoclave is 80%, and the autoclave is placed in a 160°C oven to react for 12 hours. After cooling to room temperature, the collected products are respectively Ultrasonic cleaning 3 times with deionized water and ethanol, and then drying to obtain bismuth oxychloride samples;
[0016] (2) Preparation of bismuth iodide oxide: Weigh 0.5g of bismuth nitrate pentahydrate and 0.171g of potassium iodide and mix in a beaker filled with deionized water, stir the mixture at room temperature for 30min, seal the beaker with a film, and place at 80°C React in a water bath for 2 hours, after cooling to room temperature, was...
Embodiment 2
[0019] (1) Preparation of bismuth oxychloride with flake structure: Weigh 0.5g of bismuth nitrate pentahydrate and 0.077g of potassium chloride and mix them in a beaker filled with deionized water, then stir the mixture at room temperature for 30min, and finally transfer to In a 25ml airtight autoclave containing polytetrafluoroethylene lining, the filling volume of the autoclave is 80%, and the autoclave is placed in a 160°C oven to react for 12 hours. After cooling to room temperature, the collected products are respectively Ultrasonic cleaning 3 times with deionized water and ethanol, and then drying to obtain bismuth oxychloride samples;
[0020] (2) Preparation of bismuth iodide oxide: Weigh 0.5g of bismuth nitrate pentahydrate and 0.171g of potassium iodide and mix in a beaker filled with deionized water, stir the mixture at room temperature for 30min, seal the beaker with a film, and place at 80°C React in a water bath for 2 hours, after cooling to room temperature, was...
Embodiment 3
[0023] (1) Preparation of bismuth oxychloride with flake structure: Weigh 0.5g of bismuth nitrate pentahydrate and 0.077g of potassium chloride and mix them in a beaker filled with deionized water, then stir the mixture at room temperature for 30min, and finally transfer to In a 25ml airtight autoclave containing polytetrafluoroethylene lining, the filling volume of the autoclave is 80%, and the autoclave is placed in a 160°C oven to react for 12 hours. After cooling to room temperature, the collected products are respectively Ultrasonic cleaning 3 times with deionized water and ethanol, and then drying to obtain bismuth oxychloride samples;
[0024] (2) Preparation of bismuth iodide oxide: Weigh 0.5g of bismuth nitrate pentahydrate and 0.171g of potassium iodide and mix in a beaker filled with deionized water, stir the mixture at room temperature for 30min, seal the beaker with a film, and place at 80°C React in a water bath for 2 hours, after cooling to room temperature, was...
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