Efficient and safe preparation method for active carbon material for adsorbing phosphorus in water body
An activated carbon and safe technology, which is applied in the field of activated carbon materials and preparations for efficient and safe adsorption of phosphorus in water bodies, can solve problems such as inability to use phosphorus in drinking water, hidden environmental safety hazards, and environmental pollution, and prevent plant branches and leaves from withering and re-staining water bodies. Secondary pollution and high treatment efficiency
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Embodiment 1
[0024] Dry Zailihua naturally for seven days, chop the raw materials, grind them into powder, pass through a sieve with a sieve aperture of 1mm, and put them in an oven at 105°C for three hours; then put them into a carbonization furnace with nitrogen gas for high-temperature carbonization, and the heating rate is divided into 5°C / min, heat up to 500°C, keep warm for two hours, and cool to room temperature. Introduce carbon dioxide gas for high-temperature activation, the heating rate is 5°C / min, and the temperature is raised to 600°C, kept for two hours, and cooled to room temperature. The specific surface area of the final product reaches 287.95m 2 / g, calcium content 18.10g / kg, magnesium content 3.43g / kg.
[0025] The adsorption effect takes the experiment of activated carbon product adsorption of phosphorus in water as an example.
Embodiment 2
[0027] Weigh 0.2g of activated carbon sample, place it in a 500ml Erlenmeyer flask, add 50ml of 1mg / L KH with different initial concentrations 2 PO4 solution, three replicates for each sample, placed in a constant temperature shaker, shaken at 120r / min, 25°C for 48h, filtered, pipette the supernatant, and use the molybdenum blue colorimetric method to analyze and calculate the phosphorus in the remaining solution After testing, the phosphorus removal rate of activated carbon products reached 70.30%.
Embodiment 3
[0029] Weigh 0.2g of activated carbon sample, place it in a 500ml Erlenmeyer flask, add 50ml of KH with different initial concentrations of 2mg / L 2 PO4 solution, three replicates for each sample, placed in a constant temperature shaker, shaken at 120r / min, 25°C for 48h, filtered, pipette the supernatant, and use the molybdenum blue colorimetric method to analyze and calculate the phosphorus in the remaining solution After testing, the removal rate of phosphorus by activated carbon products reached 79.17%.
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