Preparation method of ophoipogon japonicus extract and application thereof in cigarettes

A technology of Ophiopogon japonicus extract and Ophiopogon japonicus, which is applied in the extraction and application fields of natural plants, can solve the problems of inconsistent smoking sensation of cigarettes, excessive flakes and expanded cut tobacco, and deteriorated cigarette aroma quality, etc., so as to improve the quality of tobacco. Taste, ease of implementation, effect of improving tobacco aroma

Active Publication Date: 2015-01-21
CHINA TOBACCO FUJIAN IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, after applying these coke reduction technologies, the quality of cigarettes will often change significantly. For example, if the air permeability of cigarette paper is too large, the smoking experience will be inconsistent before and after the cigarette; if the ventilation of the filter is too high, the style of the cigarette will change greatly and the taste will be dry; There are too many flakes and expanded shredded tobacco, and the aroma quality of cigarettes deteriorates. Therefore, the key point and difficulty in the development and design of low-tar cigarette products is not simply reducing the tar content of cigarettes, but lies in the application of comprehensive tar reduction technology to reduce the total amount of tar in cigarettes. , also maintain a good smoking style of cigarette products, so that consumers can get psychological and physical satisfaction while improving smoking safety

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] A preparation method of Ophiopogon japonicus extract and its application in cigarettes, the steps are as follows:

[0017] 1. Crush Ophiopogon japonicus medicinal material to 80 meshes, weigh 1Kg Ophiopogon japonicus Ophiopogon japonicus powder, heat and reflux extract once with 8 times the amount of 95% ethanol for 3 hours each time, filter, combine filtrates, and concentrate under reduced pressure to obtain a concentrated solution .

[0018] 2. Adsorb the concentrated solution on an AB-8 macroporous resin column (the ratio of medicinal material / resin is 1:2), first elute with water for 3 column volumes, and then use 40% ethanol for 3 column volumes, and collect 40% The ethanol eluted part is recovered, concentrated and dried to obtain the Ophiopogon japonicus extract.

[0019] 3. Take the Ophiopogon japonicus extract prepared above and dissolve it with 10 parts of water to prepare a dilution; take the dilution that accounts for 0.01% of the cut tobacco weight and add...

Embodiment 2

[0023] A preparation method of Ophiopogon japonicus extract and its application in cigarettes, the steps are as follows:

[0024] 1. Pulverize the Ophiopogon japonicus medicinal material to 80 meshes, weigh 1Kg Ophiopogon japonicus Ophiopogon japonicus powder, heat and reflux extraction with 15 times the amount of water for 3 times, each time for 1 hour, filter, combine the filtrates, and concentrate under reduced pressure to obtain a concentrated solution;

[0025] 2. Adsorption on HP-20 macroporous resin column on the concentrated solution (medicine material / resin ratio is 1:2), first eluted with water for 3 column volumes, then eluted with 20% ethanol for 3 column volumes, collected 20% The ethanol eluted part is recovered, concentrated and dried to obtain the Ophiopogon japonicus extract.

[0026] 3. Take the Ophiopogon japonicus extract prepared above and dissolve it with 10 parts of water to prepare a dilution; take the dilution which accounts for 0.03% of the cut tobacc...

Embodiment 3

[0030] A preparation method of Ophiopogon japonicus extract and its application in cigarettes, the steps are as follows:

[0031] 1. Grind the Ophiopogon japonicus medicinal material to 80 mesh, weigh 2Kg Ophiopogon japonicus Ophiopogon japonicus powder, heat and reflux extract with 10 times the amount of 30% ethanol twice, for 2 hours each time, filter, combine the filtrates, and concentrate under reduced pressure to obtain concentrated liquid;

[0032] 2. The concentrate is adsorbed on a HPD100 macroporous resin column (the ratio of medicinal material / resin is 1:5). First, 3 column volumes are eluted with water, and then 3 column volumes are eluted with 30% ethanol, and the 30% ethanol wash is collected. Partially removed, ethanol recovered, concentrated and dried to obtain the Ophiopogon japonicus extract.

[0033] 3. Take the Ophiopogon japonicus extract prepared above and dissolve it with 75% ethanol to prepare a dilution; take the dilution that accounts for 0.03% of the...

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PUM

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Abstract

The invention discloses a preparation method of ophoipogon japonicus extract and the application of the ophoipogon japonicus in cigarettes. The ophoipogon japonicus is used as raw materials and obtained by means of the extractive method as the following steps: extracting a concentrated solution with ethonal or water after drying the ophoipogon japonicus herbs; eluting and purifying the concentrated solution with a macroporous resin column; and concentrating, cooling and drying the eluted and purified solution. Therefore, the ophoipogon japonicus extract is obtained. Due to the fact that the ophoipogon japonicus extract is used as a cigarette additive to be added into cut tobacco of the cigarette, woody gas, irritant sense and dry sense of the cigarette can be obviously improved, aroma is enabled to be soft and moist, the secretion of salvia or body fluid is promoted, sweetness is enhanced, and fragrant of the cigarette is enabled to be coordinated. Due to the fact that the ophoipogon japonicus is extracted and purified by means of ethonal or an ethonal-water solution and microporous resin, the preparation method of the ophoipogon japonicus extract and application of the ophoipogon japonicus in the cigarette have the advantages of being simple in extraction process, easy and convenient to operate, explicit in extractable content, and capable of providing extracts of natural plants which are novel and good in effect for improving taste of tobacco.

Description

technical field [0001] The present invention relates to the extraction and application of a natural plant, in particular to the preparation of Ophiopogon japonicus extract and its application in cigarettes. Background technique [0002] Cigarettes are a special consumer product with a stubborn hobby. The smoking taste and safety of cigarette products are the most important factors that determine consumers' choice to buy. Cigarette smoking taste refers to consumers' feelings on the type, intensity and aroma of cigarettes they smoke. my country has a large population, a vast territory, and great differences in economic level, climatic conditions, and consumption habits. As a result, the smoking tastes of cigarette consumption in my country are relatively complicated. Consumers' smoking tastes vary greatly between different regions, showing a regional distribution of smoking tastes. Diversified features. [0003] Although a variety of cigarette flavor styles have been formed a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B9/00A24B15/30A24B3/12
Inventor 蓝洪桥陈小明李斌林凯洪祖灿邱彦
Owner CHINA TOBACCO FUJIAN IND
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