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Optical fiber perform doper and doping method

A technology of optical fiber preform and heating evaporation, which is applied in the direction of manufacturing tools and glass manufacturing equipment, can solve the problems of large background loss, high cost, complex technology, etc., to ensure consistency and uniformity, prevent condensation and pre-reaction, The effect of simplifying the manufacturing process

Inactive Publication Date: 2013-10-23
XI'AN INST OF OPTICS & FINE MECHANICS - CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the solution doping technology has the advantages of simple operation and high flexibility, with the continuous rise of other doping technologies and technical optimization, the use of this method to dope rare earth ions in optical fibers has increasingly shown its limitations. The main performance In: large background loss, poor repeatability, low doping concentration, poor uniformity, uneven refractive index distribution, easy crystallization of the fiber core, difficulty in increasing the size of the core rod, long production cycle, low efficiency, and high cost.
The doping concentration of the chloride gas-phase doping method and the sol-gel meth

Method used

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  • Optical fiber perform doper and doping method
  • Optical fiber perform doper and doping method
  • Optical fiber perform doper and doping method

Examples

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example 1

[0064] The preparation of the ytterbium-doped optical fiber preform of example 1 core diameter 2mm

[0065] First the polishing dry gas SF 6 and Cl 2 Pass into the quartz deposition tube 201, adjust the temperature of the heating torch 203 to polish and dry the deposition tube 201; then the substrate deposition gas SiCl 4 , O 2 , SF 6 , He is passed into the quartz deposition tube 201 from the conduit interface 204, and the temperature of the heating torch 203 is set between 1350-1850°C. In this embodiment, the temperature of the heating torch 203 is selected to be adjusted at 1550°C, and 6 layers of SiO are deposited. 2 The powder layer is used as the cladding part of the optical fiber preform, deposited for 1.5 hours; then the matrix is ​​deposited with gas SiCl 4 , O 2 , SF 6 , He, POCl 3 While passing into the quartz deposition tube 201 from the conduit interface 204, adjust the temperature of the heating evaporation tank 105 to be 210° C., the flow rate of the carr...

example 2

[0071] The preparation of the ytterbium-doped optical fiber preform of example 2 core diameter 4mm

[0072] First the polishing dry gas SF 6 and Cl 2 Pass into the quartz deposition tube 201, adjust the temperature of the heating torch 203 to polish and dry the deposition tube 201; then the substrate deposition gas SiCl 4 , SF 6 , O 2 , He, Cl 2 , POCl 3 Pass it into the quartz deposition tube 201, set the temperature of the heating torch 203 between 1450-1750°C, and adjust the temperature of the heating torch 203 at 1600°C in this embodiment, and deposit 8 layers of SiO 2 The powder layer is used as the cladding part of the optical fiber preform, deposited for 2 hours; then the matrix is ​​deposited with gas SiCl 4 、GeCl 4 , SF 6 , O 2 , He, POCl 3While passing through the quartz deposition tube 201, set the temperature of the two heating evaporation tanks 105 at 200°C and 220°C respectively, and adjust the flow rate of the flow controller of the corresponding air i...

example 3

[0079] Preparation of ytterbium-doped optical fiber preform with core diameter 7mm of example 3

[0080] First the polishing, drying gas SF 6 and Cl 2 Pass into the quartz deposition tube 201, adjust the temperature of the heating torch 203 to polish and dry the deposition tube 201; then the substrate deposition gas SiCl 4 , SF 6 , O 2 , He, Cl 2 、BBr 3 Pass it into the quartz deposition tube 201, set the temperature of the heating torch 203 between 1550-1850°C, and adjust the temperature of the heating torch 203 at 1650°C in this embodiment, and deposit 6 layers of SiO 2 The powder layer is used as the cladding part of the optical fiber preform, deposited for 1.5 hours; then the matrix is ​​deposited with gas SiCl 4 、GeCl 4 , SF 6 , O 2 , He is passed into the quartz deposition tube 201, and the temperatures of the two heating evaporation tanks 105 are respectively set at 100°C and 210°C, and the flow rate of the flow controller of the corresponding air inlet conduit...

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Abstract

The invention provides an optical fiber perform doper and a doping method. The optical fiber perform doper comprises a heating system, a transmission system and an improved chemical vapor deposition system. The heating system comprises heating evaporators and air-intake ducts and air-outlet ducts which communicate with the heating evaporators. The transmission system comprises a heating and heat preservation transmission pipe and a heating and heat preservation plate. An oxygen pipe used for inletting high-purity oxygen and the air-outlet ducts are respectively accessed into the heating and heat preservation transmission pipe provided with corresponding interfaces. An output end of the heating and heat preservation transmission pipe communicates with a rotating part of the improved chemical vapor deposition system. Different organic metal chelates are placed in each heating evaporator, wherein an organic metal chelate in at least one of the heating evaporators is used as a doping agent. With the application of the doper provided by the invention, all gas-phase doping can be realized, and heat preservation during the whole course makes gases not to be easily coagulated. By the adoption of the doping method, doping uniformity and consistency of the product are both raised, and performance of the product is also guaranteed appropriately.

Description

technical field [0001] The invention belongs to optical fiber preparation technology, and relates to an optical fiber preform doping device and method thereof, in particular to an all-gas optical fiber preform doping device and method using an organic metal chelate as a dopant and a co-dopant . Background technique [0002] Rare earth-doped special fibers are widely used in fiber lasers, amplifiers and sensors, and have been greatly developed in recent years. The dopants used are Nd, Er, Ge, Pr, Ho, Eu, Yb, Dy , Tm and other elements with atomic numbers ranging from 57 to 71 can be individually doped with a certain rare earth element for single doping, or jointly doped with multiple rare earth elements for co-doping. It is characterized by a cylindrical waveguide structure, small core diameter, easy to achieve high-density pump lasing, low threshold value, large surface area, good heat dissipation performance, its core diameter matches communication optical fiber, high coup...

Claims

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Application Information

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IPC IPC(8): C03B37/018
Inventor 林傲祥师腾飞倪立张爱东湛欢李璐何建丽周志广
Owner XI'AN INST OF OPTICS & FINE MECHANICS - CHINESE ACAD OF SCI
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