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Method for solving large pressure difference of iron-molybdenum catalyst in iron-molybdenum converter

A solution and converter technology, which is applied to the solution field of iron-molybdenum catalyst with large pressure difference in iron-molybdenum converter, can solve the problems of large pressure difference and slow speed of iron-molybdenum catalyst

Active Publication Date: 2015-02-11
QITAIHE BAOTAILONG METHANOL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The present invention is to solve the problem that the existing iron-molybdenum catalyst has a large pressure difference and needs to be regenerated under the condition of parking, and the speed is slow, and solves the problem of the large pressure difference of the iron-molybdenum catalyst in the iron-molybdenum converter
[0004] The method for solving the iron-molybdenum catalyst pressure difference in the iron-molybdenum converter of the present invention is carried out according to the following steps:

Method used

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  • Method for solving large pressure difference of iron-molybdenum catalyst in iron-molybdenum converter
  • Method for solving large pressure difference of iron-molybdenum catalyst in iron-molybdenum converter
  • Method for solving large pressure difference of iron-molybdenum catalyst in iron-molybdenum converter

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specific Embodiment approach 1

[0018] Specific embodiment one: the regeneration method of iron-molybdenum catalyst in the iron-molybdenum converter of the present embodiment is carried out according to the following steps:

[0019] 1. The iron-molybdenum conversion system includes a heating furnace 1, an iron-molybdenum converter 2, the first coke oven gas pipe 3, the second coke oven gas pipe 4, the fuel gas pipe 5 and the vent pipe 6;

[0020] The heating furnace 1 is composed of a furnace 1-1, a flue 1-2 and a coil 1-3; the coil 1-3 is located in the furnace 1-1, and the flue 1-2 is located at the top of the heating furnace 1; in the flue 1- Butterfly valve 1-2-1 is set on 2; a furnace door 1-1-1 is opened on the side wall of furnace 1-1, and fuel gas burner 1-1-2 is installed at the bottom of furnace 1-1;

[0021] The interior of the iron-molybdenum converter 2 is provided with upper and lower layers of iron-molybdenum catalyst beds 2-1, a coke oven gas inlet 2-2 is arranged on the top of the iron-molyb...

specific Embodiment approach 2

[0030] Embodiment 2: This embodiment differs from Embodiment 1 in that: in Step 5, the temperature of the coke oven gas at the exit of the coil 1-3 is 396-398°C. Others are the same as the first embodiment.

specific Embodiment approach 3

[0031] Specific embodiment three: the difference between this embodiment and specific embodiment one or two is that in step five, the coke oven gas is passed into the iron-molybdenum converter 2 of normal operation to mix with the coke oven gas in the second coke oven gas pipe 4, mix The temperature of post-coke oven gas is controlled at 360-370°C. Others are the same as in the first or second embodiment.

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Abstract

The invention relates to a method for solving large pressure difference of an iron-molybdenum catalyst in an iron-molybdenum converter, relates to a method for regenerating the iron-molybdenum catalyst, and is used for solving the problem that the stop treatment needs to be carried out and the treatment speed is low when the pressure difference of the existing iron-molybdenum catalyst is large. According to the method, an iron-molybdenum converting system comprises a heating furnace, the iron-molybdenum converter, a first coke oven gas pipe, a second coke oven gas pipe, a fuel gas pipe and an escape pipe; after coke oven gas is fed in the heating furnace and is heated to 400 DEG C, the coke oven gas is mixed with the coke oven gas in the normally running iron-molybdenum converter together to be fed in the iron-molybdenum converter, so that an iron-molybdenum bed is heated till the hot-spot temperature of the bed is 450-500 DEG C; impurities such as coil tar oil and benzene adhered on the surface of the iron-molybdenum catalyst are melted and move downwards, so that the pressure difference of the catalyst bed is reduced, and then the temperature of the iron-molybdenum catalyst bed is reduced to the level of normal production. The method is performed under the condition that facilities such as equipment, pipelines and valves of a fine desulfurization system are not changed, and the pressure difference of the iron-molybdenum catalyst is reduced without stopping production.

Description

technical field [0001] The invention relates to a solution to the large pressure difference of the iron-molybdenum catalyst. Background technique [0002] Since the coke oven gas contains coal tar, dust, naphthalene, benzene and other impurities, after the wet desulfurization section, the compression section, the oil filter for fine desulfurization and the pre-desulfurization tank, the tar, naphthalene, and benzene in the coke oven gas still cannot Benzene is completely removed, causing some impurities to enter the iron-molybdenum converter, tar adsorbed on the surface of the catalyst, and accumulates for a long time, which increases the pressure difference between the inlet and outlet of the iron-molybdenum converter, and increases the resistance of compressed and transported gas for fine desulfurization conversion, causing coke The load of the furnace gas compressor increases, the valve plate is easily damaged, and the system is forced to stop to replace the catalyst and t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J38/02
Inventor 边兴海秦怀张波李怀建刘家兴王新嘉张宏王晓飞赫长坤张福友王中兴张丽
Owner QITAIHE BAOTAILONG METHANOL