Liquid crystal aligning agent for photo-alignment treatment method, and liquid crystal aligning film using the liquid crystal aligning agent
A technology of liquid crystal alignment agent and liquid crystal alignment film, applied in optics, nonlinear optics, instruments, etc., can solve the problem of insufficient stability of alignment control force
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[0242] The following examples are given to illustrate the present invention more specifically, but the present invention is not limited thereto. In addition, the abbreviations of the compounds used in the present Examples and Comparative Examples and the measurement methods of each characteristic are as follows.
[0243] NMP: N-methyl-2-pyrrolidone
[0244] BCS: Butyl Cellosolve
[0245] GBL: gamma-butyrolactone
[0246] AIBN: 2,2'-azobisisobutyronitrile
[0247] DA-1: the following formula (DA-1)
[0248] DA-2: the following formula (DA-2)
[0249] MA1: following formula (MA-1)
[0250]
[0251] [viscosity]
[0252] In the synthesis example, the viscosity of the polyamic acid ester and the polyamic acid solution was measured using an E-type viscometer TVE-22H (manufactured by Toki Sangyo Co., Ltd. (Toki Sangyo Co., Ltd.)) with a sample volume of 1.1 mL and a conical rotor TE-1 ( 1°34', R24) and temperature 25°C.
[0253] [molecular weight]
[0254] In addition, th...
Synthetic example 1)
[0266] 2394 g of NMP was added to a 3000 mL four-necked flask equipped with a stirring device and a nitrogen gas introduction tube, and 196.34 g (1.00 mol) of 1,2,3,4-cyclobutanetetracarboxylic dianhydride was added. While stirring the slurry of tetracarboxylic dianhydride, add 101.11g (0.935mol) of p-phenylenediamine, then add NMP to make the solid content concentration 8% by mass, and stir at room temperature for 24 hours to obtain polyamic acid (PAA- 1) solution. The viscosity of this polyamic acid solution at a temperature of 25° C. was 115 mPa·s.
Synthetic example 2)
[0268] Take 5.73g (20.0mmol) of 1,5-bis(4-aminophenoxy)pentane in a 100mL four-necked flask with a stirring device and a nitrogen inlet tube, add 65.4g of NMP, and stir while delivering nitrogen. Let it dissolve. While stirring this diamine solution, add 4.19 g (19.2 mmol) of pyromellitic dianhydride, then add NMP so that the solid content concentration becomes 12% by mass, and stir at room temperature for 24 hours to obtain polyamic acid (PAA-2). The solution. The viscosity of this polyamic acid solution at a temperature of 25° C. was 520 mPa·s.
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