A kind of preparation method of neodymium-based multi-ligand rubber vulcanization accelerator

A rubber vulcanization, multi-ligand technology, applied in chemical instruments and methods, organic chemistry, compounds containing elements of Group 3/13 of the periodic table, etc., can solve problems such as poor solubility, simplify the process and improve the solubility. The effect of sex and consumption saving
CN103819716BActive Publication Date: 2016-02-10BEIJING UNIV OF CHEM TECH
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
BEIJING UNIV OF CHEM TECH
Publication Date
2016-02-10

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Abstract

The invention discloses an Nd-based multi-ligand vulcanization accelerator and a preparation method thereof. In synthesis, an Nd element is used as a rare earth element, and four ligands are contained; the ligand 1 and the ligand 2 are accelerator radicals with good vulcanization acceleration effects, the ligand 3 is phenanthroline capable of forming strong coordination with the rare earth element, and the ligand 4 is acrylic acid capable of improving the solubility of the accelerator in a sizing material. The preparation method is simple, convenient and feasible, does not need inert gas shielding, is mild in preparation process condition, and has no harmful gas generation. The multi-ligand rare earth vulcanization accelerator has good solubility in rubber, and is long in vulcanization and scorching time, good in vulcanization curve flatness, non-toxic, odorless and pollution-free. The vulcanization accelerator can replace a currently used zinc oxide, stearic acid and accelerator combination system, and is applicable to high performance tires and other rubber products.
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Description

technical field

[0001] The invention relates to a synthesis method of a neodymium-based multi-ligand vulcanization accelerator and research on its vulcanization acceleration effect. This accelerator does not need zinc oxide and stearic acid as an activator, and has the advantages of saving the feeding process, clean and pollution-free, good vulcanization flatness, and easy to uniformly disperse in rubber. The rubber composite material prepared by using this accelerator has the advantages of Good performance uniformity. Background technique

[0002] The vulcanization system of rubber is a complete vulcanization system composed of accelerators, activators, and vulcanizing agents. Among them, the accelerator is a chemical substance that can shorten the vulcanization time, lower the vulcanization temperature, reduce the amount of vulcanizing agent, and improve and improve the physical and mechanical properties and chemical stability of the vulcanized rubber. Just because accel...

Claims

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