Polyimide photosensitive resin composition for organic light emitting diode
A technology of photosensitive resin and polyimide, which is applied in the field of polyimide photosensitive resin composition, can solve problems such as low sensitivity, difficulty in adjusting molecular weight and solubility, and reduced yield, and achieve the effect of improving sensitivity
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Embodiment 1
[0092] (Manufacture of polyimide precursor)
[0093] In a 300 ml 4-port reaction vessel, 4 g of DADM (chemical formula 5), 7 g of Bis-APAF (chemical formula 6), and 1 g of SiDA (chemical formula 7) were dissolved with 70 g of γ-butyrolactone. In addition, 5 g of 6-FDA (chemical formula 2), 3 g of DOCDA (chemical formula 3), and 3 g of a-BPDA (chemical formula 4), which are dianhydrides, were put into a reaction vessel, stirred and reacted for 1 hour. In order to terminate the reaction at the end, after adding 2g of PA, an additional reaction time was added at 20°C for 1 hour, and a polyimide precursor with a solid content of 30% was produced. After adding 5 g of ECMMA and MGMA as a protective substance and adding 10 g in total to this, TEA was added as a catalyst after heating up to 70° C., and reacted for 24 hours to manufacture a new polyimide precursor.
[0094] (Manufacture of polyimide photosensitive resin composition for OLED)
[0095] 30 parts by weight of the polyi...
Embodiment 2
[0097] In said Example 1, except having used ECMMA10g at the time of manufacture of a polyimide precursor, it implemented by the method similar to said Example 1, and manufactured the polyimide photosensitive resin composition for OLEDs.
Embodiment 3
[0099] In said Example 1, except having used MGMA10g instead of ECMMA, the polyimide photosensitive resin composition for OLED was manufactured by the method similar to said Example 1.
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