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Suspended rotary catalyst ageing oven

An aging furnace and catalyst technology, which is applied in the preparation of test samples and other directions, can solve the problems of poor manufacturability, high precision required for coaxiality, and reduced operating safety of the device, and achieves low cost, increased safety, and compact structure. Effect

Inactive Publication Date: 2014-08-27
KYMSON LUOYANG PETROCHEM EQUIP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this method adopts the method of entering water vapor from the upper part, and there is a back-mixing phenomenon of water vapor in the roaster, and the exhaust gas generated by the aging of the sample will affect the sample; the rotating shaft is supported by the upper and lower ends, and the support points are far apart. Requires high precision and poor workmanship; in addition, two high-temperature sealing points reduce the safety of device operation

Method used

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  • Suspended rotary catalyst ageing oven
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  • Suspended rotary catalyst ageing oven

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] Aging results of the same catalyst sample in different sample cups

[0041]In 12 sample cups made of 60 ml porous ceramic materials, 40 grams of MLC-500 industrial fresh full sieve (0-150 μm) catalysts were all filled, under 100% water vapor, the aging temperature was 800 ° C, and the aging time was 17 hours. Under the condition that the pressure is normal pressure, the influence of the microreactive activity after aging of 12 (one layer) samples in the rotary aging furnace was investigated. The results are shown in Table 1.

[0042] Table 1 Microreactive activity after rotation aging under the same conditions

[0043]

Embodiment 2

[0045] Effect of Catalyst Packing Thickness on Aging Results

[0046] In 6 sample cups made of 60 milliliters of porous ceramic materials, fill respectively 15, 20, 25, 30, 35, 40 grams of MLC-500 industrial fresh full screening (0 ~ 150 μm) catalyst, under 100% steam, Under the condition of aging temperature of 800℃, aging time of 17 hours and normal pressure, the effect of catalyst packing thickness on aging results was investigated. The results are shown in Table 2.

[0047] Table 2 Effect of catalyst packing thickness on aging results

[0048]

Embodiment 3

[0050] Rotation Aging Repeatability Investigation Test Results

[0051] The loading of the catalyst is 30 grams, 800° C., 100% water vapor, aging for 17 hours, and the pressure is normal pressure. The test results are shown in Table 3.

[0052] Table 3 Rotation aging repeatability inspection test results

[0053]

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Abstract

The invention relates to a suspended rotary catalyst ageing oven, comprising a feeding pipe, temperature measuring pipes, an ageing oven, a sample cup bracket, a sample cup, a rotating shaft, a radiator, supporting rods, a motor, a cylinder fixing plate, a lifting cylinder, lifting guide rails, a connecting plate, a motor support frame, a steam outlet pipe and a flange, wherein the upper end of the rotating shaft is connected with the motor and then passes through the center of the flange, the lower end of the rotating shaft is connected with the center of the sample cup bracket, the sample cup is arranged on the sample cup bracket, the motor is supported and fixed by the motor support frame which is fixed on the flange, the flange is fixed on the connecting plate through the two supporting rods, the lifting cylinder is fixed on the cylinder fixing plate, the upper ends of the lifting guide rails are fixed on the cylinder fixing plate, the lower ends of the lifting guide rails are fixed on the flange, the feeding pipe is located at the bottom end of the aging oven, the steam outlet pipe in located between the connecting plate and the flange, the radiator is arranged on the rotating shaft, and the temperature measuring pipes are arranged between the bottom end of the aging oven and the flange.

Description

technical field [0001] The invention relates to a catalyst aging furnace, in particular to an aging furnace for evaluating the hydrothermal stability of molecular sieves, catalysts, etc., which is used for catalyst aging in a laboratory. Background technique [0002] Catalysts are widely used in petroleum, chemical and other fields. Many catalytic processing processes are completed under the action of catalysts. The performance of the catalyst directly affects the product yield and product quality. Therefore, it is very important to develop and research catalysts with superior performance. In the process of catalyst research and development, the evaluation of catalyst performance and other properties requires various experimental devices and process methods, and the aging of catalysts is the first step in various evaluations of catalysts. [0003] Such as catalytic cracking fresh catalyst activity is high and unstable, not representative. When researching and evaluating c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/44
Inventor 秦晨晨王翀王广亮王义坤陈宾冯川
Owner KYMSON LUOYANG PETROCHEM EQUIP
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