Method for preparing nanogold through mango peel reducing agent

A mango peel and reducing agent technology, applied in the field of biotechnology and nano research, can solve the problems of environmental and biological hazards, large toxic and side effects, and environmental pollution, and achieve the effect of not easy to reunite, simple steps, and good dispersion

Inactive Publication Date: 2014-10-01
SHANXI AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Both physical and chemical methods have the following problems: (1) relatively strict conditions are required; (2) high energy consumption; (3) the reagents used are expensive and have large toxic and side effects; biohazardous
However, the current processing status has not been utilized, and most of the mango peels are discarded, which not only causes a huge waste of resources, but also pollutes the environment

Method used

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  • Method for preparing nanogold through mango peel reducing agent
  • Method for preparing nanogold through mango peel reducing agent
  • Method for preparing nanogold through mango peel reducing agent

Examples

Experimental program
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Effect test

Embodiment 1

[0027] Nano gold is prepared by the method of the invention.

[0028] (1) Preparation of chloroauric acid solution First weigh 0.041g of chloroauric acid powder and dissolve it in 100mL of distilled water to obtain 1mmol of chloroauric acid solution. Since chloroauric acid is highly corrosive, metal medicines should not be used during operation. spoon, then adjust the pH value of the chloroauric acid solution to 9.0 with aqueous sodium hydroxide solution;

[0029] (2) Preparation of mango peel reducing agent Take fresh mango peel and wash it with distilled water for 3 times, dry it in an oven at 80°C, then crush it to 100 mesh, put it in a ziplock bag for later use;

[0030] (3) Preparation of gold nanoparticles Measure 50mL of the chloroauric acid solution prepared in (1), add 3g of the mango peel reducing agent prepared in (2), stir well, and bathe in water for 100min at 25°C, observe the color of the solution. When the acid solution changes from yellow to purple, the react...

Embodiment 2

[0033] Nano gold is prepared by the method of the invention.

[0034] (1) Preparation of chloroauric acid solution First weigh 0.041g of chloroauric acid powder and dissolve it in 100mL of distilled water to obtain 1mmol of chloroauric acid solution, then adjust the pH value of the chloroauric acid solution to 7.0 with sodium hydroxide aqueous solution;

[0035] (2) Preparation of mango peel reducing agent Take fresh mango peel and wash it twice with distilled water, freeze-dry it under vacuum at -80°C, take the freeze-dried powder and grind it through a 100-mesh sieve, put it in a ziplock bag for later use;

[0036] (3) Preparation of gold nanoparticles Measure 50 mL of the chloroauric acid solution prepared in (1), add 1 g of the mango peel reducing agent prepared in (2), stir well, and bathe in water at 30°C for 90 minutes, observe the color of the solution, when the gold chloride When the acid solution changes from yellow to purple, the reaction is terminated; the purple-r...

Embodiment 3

[0039] Nano gold is prepared by the method of the invention.

[0040](1) Preparation of chloroauric acid solution First weigh 0.041g of chloroauric acid powder and dissolve it in 100mL of distilled water to obtain 1mmol of chloroauric acid solution, then adjust the pH value of the chloroauric acid solution to 8.0 with sodium hydroxide aqueous solution;

[0041] (2) Preparation of mango peel reducing agent Wash fresh mango peel with distilled water for 3 times, dry naturally, crush and pass through a 100-mesh sieve, then mix fresh mango peel: ethanol: water volume ratio of 1:1.5:1.5 and reflux Extract for 3 hours, and store the extract in a 4°C refrigerator for later use;

[0042] (3) Preparation of gold nanoparticles Measure 50 mL of the chloroauric acid solution prepared in (1), add 10 mL of mango peel reducing agent extract prepared in (2), stir well, put in a water bath at 28°C for 95 minutes, and observe the color of the solution , when the chloroauric acid solution chang...

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Abstract

The invention provides a method for preparing nanogold through a mango peel reducing agent. The method comprises the following steps: preparing a chloroauric acid solution; adjusting the pH value of the chloroauric acid solution; adding a mango peel reducing agent accounting for 2%-20% of the chloroauric acid solution according to volume ratio; performing water bath for 90-100 min under a certain condition; stopping the reaction when the color of the chloroauric acid solution turns into fuchsia from yellow; separating composite nanogold from the chloroauric acid solution through centrifugal separation; lastly, washing subnatant with distilled water and dehydrating; drying the the subnatant obtained through separation under a certain condition to obtain nanogold particles. According to the method, as the mango peels are prepared into as the reducing agent, the mango peels are changed from waste into valuable and the comprehensive utilization benefits of mangos are increased; compared with the prior art, the method has the advantages that steps are simple, the condition is mild, the preparing steps are simplified greatly and difficulties are reduced; no poisonous by-products are generated in the synthesizing processes, the yield of prepared nanogold particles can reach 90% above; the composite nanogold particles are even in sizes, narrow in particle size distribution, good in dispersity, low in possibility of gathering and more stable.

Description

technical field [0001] The invention relates to the field of biotechnology and nanometer research, in particular to a method for preparing nano gold by treating mango skin into a reducing agent and chloroauric acid. Background technique [0002] At present, the methods for preparing nano gold are mainly physical and chemical methods. The physical method refers to the direct conversion of gold into nanoparticles through various dispersion techniques; the chemical method refers to the reduction reaction of gold compounds to obtain nanoparticles. Both physical and chemical methods have the following problems: (1) relatively strict conditions are required; (2) high energy consumption; (3) the reagents used are expensive and have large toxic and side effects; (4) environmental pollution is relatively serious, which is harmful to the environment and Living organisms pose a potential hazard. With the popularity of the concept of green chemistry, the synthesis of gold nanoparticle...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F9/24B82Y40/00
Inventor 杨宁李维宏
Owner SHANXI AGRI UNIV
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