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A kind of polymerization reactor component and its using method

A technology for a polymerization reaction kettle and an assembly is applied in the field of the reaction kettle assembly and its control process, which can solve the problems of high labor intensity for operators in manual cleaning, large pressure difference between the upper and lower rubber blocks, affecting production efficiency, etc. The effect of reducing design pressure and improving efficiency

Active Publication Date: 2017-09-29
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Nevertheless, under some specific polymer conditions, the extrusion of colloidal polymers is sometimes difficult to carry out, especially high molecular weight polyacrylamide colloidal polymers, sometimes due to excessive friction between the wall of the kettle and the overall rubber block And the air pressure applied in the kettle is relatively high (0.3-0.6MPa), and the pressure at the screw machine at the discharge port is normal pressure, which causes the pressure difference between the upper and lower sides of the rubber block to be too large, causing the rubber block to be pressed through up and down, forming a perforation, and being pressed through The final rubber block loses the downward air pressure, that is, it loses the power to extrude the pulverizer to the screw below, which requires a long standing process to wait for the rubber block to gradually recover under gravity, and then continue to apply pressure for the discharge operation , Sometimes it is even necessary to disassemble the reactor for manual cleaning, which affects the production efficiency. At the same time, the manual cleaning of the operator is labor-intensive

Method used

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  • A kind of polymerization reactor component and its using method
  • A kind of polymerization reactor component and its using method
  • A kind of polymerization reactor component and its using method

Examples

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Embodiment 1

[0037] A polymerization reactor assembly and a method of use for a reaction that uses or contains acrylamide as a raw material, wherein the polymerization reactor assembly includes a kettle body 1, a gas blowing port and a gas blowing line 6, and the gas blowing port and the gas blowing line 6 Connect the gas source 10 (four groups in total), the bottom of the kettle body 1 is provided with a discharge port and connected to the granulation device, and the kettle body 1 is provided with lubricating liquid inlets 2-1, 2-2, 2-3 , 2-4, can be used for passing into lubricating liquid and purge gas, each lubricating liquid feeding port 2-1, 2-2, 2-3, 2-4 connects lubricating liquid and adds pipeline 5 to transport lubricating liquid. Each lubricating liquid adding pipeline 5 is provided with a lubricating liquid metering tank 7 , and each lubricating liquid metering tank 7 is connected to the air source 10 .

[0038] The top of the kettle body 1 is provided with a feed inlet, the bo...

Embodiment 2

[0054] The difference between embodiment 2 and the polymerization reactor assembly of embodiment 1 is:

[0055] The diameter of the straight section of kettle body 1 is φ1800mm, the length of the straight section is 3150mm, and the length of the cone section is 1300mm. Other features of the polymerization reactor assembly of Example 2 are the same as those of Example 1.

[0056] The usage method of this embodiment is as follows:

[0057] 1) Through the feeding port set on the top of the kettle body 1, add the reaction raw materials to carry out the polymerization reaction according to the requirements of the reaction process. During the polymerization reaction, use the gas blowing port and the gas blowing pipeline 6 to feed nitrogen gas to stir and mix the reaction raw materials in the kettle body 1 , after the end of the polymerization reaction, a whole block of polymer glue is formed in the kettle body 1, and the discharging operation is started;

[0058] 2) Open the disch...

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Abstract

The invention discloses a polymerization reactor assembly and a method for using the same, which are used for the reaction using or containing acrylamide as a raw material. The blowing pipeline (6) is connected to the gas source 10, the bottom of the kettle body (1) is provided with a discharge port and connected to the granulation device, and the kettle body (1) is provided with a lubricating liquid inlet (2‑1, 2‑ 2, 2‑3, 2‑4), each lubricating liquid inlet (2‑1, 2‑2, 2‑3, 2‑4) is connected to the lubricating liquid adding pipeline (5) to deliver the lubricating liquid. The introduction of lubricating liquid into the polymerization reactor assembly and its use method of the present invention reduces the resistance of the polymer being pressed out of the polymerization reactor after the polymerization reaction is completed, reduces the gas pressure required in the reactor body, and can appropriately increase the volume of the equipment. Improve efficiency, reduce energy consumption, and effectively reduce the probability of occurrence of press-through phenomenon.

Description

technical field [0001] The invention relates to a polymerization reactor component in the chemical industry and a method for using the same, in particular to a reactor component and its control process for polymerizing a colloidal high molecular polymer with or containing acrylamide as a raw material. Background technique [0002] Polyacrylamide polymers are one of a class of mass-produced water-soluble polymers. It is used in petroleum, water treatment, papermaking, textile printing and dyeing, agriculture and other fields. [0003] In the preparation of polyacrylamide products, there is a type of polyacrylamide polymerization product or copolymer that forms a whole gelatinous polymer in a polymerization reactor, with a water content of 65-80% and strong viscoelasticity. [0004] A polymer treatment process is to extrude the large colloidal polyacrylamide colloid from the bottom of the polymerization tank into a special screw extrusion pulverizer, and then pass through the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08F20/56C08F2/01
Inventor 张建新孙汝柳罗继红单薇刘莹
Owner CHINA PETROLEUM & CHEM CORP
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