Flame-retardant styrene-butadiene rubber sheath for cables and preparation method thereof
A styrene-butadiene rubber and cable technology, which is applied in the rubber field to achieve the effect of preventing the combustion reaction
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[0013] The invention provides a method for preparing a flame-retardant styrene-butadiene rubber sheath for cables, the preparation method comprising:
[0014] a. Mixing styrene-butadiene rubber, fumed silica, chlorinated paraffin, tribromophenyl acrylate, zinc borate, antimony trioxide and sodium molybdate to make masterbatch;
[0015] B, vulcanizing agent and described masterbatch are mixed to carry out vulcanization treatment for the first time;
[0016] c. Carrying out the second vulcanization of the masterbatch after the first vulcanization in an oven to make flame-retardant styrene-butadiene rubber for cables;
[0017] d. Extruding the cable with flame-retardant styrene-butadiene rubber to make a flame-retardant styrene-butadiene rubber sheath for the cable.
[0018] In the step a of the present invention, the consumption of each raw material can be selected in a wide range, but in order to make the flame-retardant styrene-butadiene rubber sheath for cables prepared has ...
Embodiment 1
[0027] a, the brand is styrene-butadiene rubber 100kg of SBS501, the brand is fumed white carbon black 180kg of A200, 5kg chlorinated paraffin-50, tribromophenyl acrylate 45kg, zinc borate 6kg, antimony trioxide 9kg and molybdic acid Mix 0.8kg of sodium to make masterbatch;
[0028] b. At 150°C and 11Mpa, mix 0.5 kg of bis-tert-butyl peroxide cumene and 100 kg of the above masterbatch for 17 minutes for the first vulcanization treatment;
[0029] c. At 215 ° C, the masterbatch after the first vulcanization is vulcanized for the second time in an oven for 4 hours to make flame-retardant styrene-butadiene rubber for cables;
[0030] d. Extrude the flame-retardant styrene-butadiene rubber for the cable to make a flame-retardant styrene-butadiene rubber sheath A1 for the cable.
[0031] The flame retardant performance parameters of the flame retardant styrene-butadiene rubber sheath for the cable are shown in Table 1.
Embodiment 2
[0033] a, the brand is styrene-butadiene rubber 100kg of SBS501, the brand is fumed white carbon black 190kg of A200, 7kg chlorinated paraffin-50, tribromophenyl acrylate 55kg, zinc borate 8kg, antimony trioxide 10kg and molybdic acid Mix 1.2kg of sodium to make masterbatch;
[0034] b. At 170°C and 12Mpa, mix 0.8 kg of bis-tert-butyl peroxide cumene and 100 kg of the above masterbatch for 20 minutes for the first vulcanization treatment;
[0035] c. At 220 ° C, the masterbatch after the first vulcanization is vulcanized for the second time in an oven for 5 hours to make flame-retardant styrene-butadiene rubber for cables;
[0036] d. Extrude the flame-retardant styrene-butadiene rubber for the cable to make a flame-retardant styrene-butadiene rubber sheath A2 for the cable.
[0037] The flame retardant performance parameters of the flame retardant styrene-butadiene rubber sheath for the cable are shown in Table 1.
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