Photosensitive resin composition and method for forming pattern using same
A technology of photosensitive resin and composition, which is applied in the field of photosensitive resin composition, can solve the problems of resolution, adhesion and residual film rate, etc., and achieve the effect of excellent characteristics and preventing greening
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Synthetic example 1
[0082] Synthesis example 1 (preparation of acrylic copolymer)
[0083] A mixed solution of 400 parts by weight of tetrahydrofuran, 30 parts by weight of methacrylic acid, 30 parts by weight of styrene, and 40 parts by weight of glycidyl methacrylate was put into a flask equipped with a cooler and a stirrer. After the liquid composition was sufficiently mixed in a mixing vessel at a speed of 600 rpm, 15 parts by weight of 2,2'-azobis(2,4-dimethylvaleronitrile) was added. The temperature of the mixed solution of the polymerization is slowly raised to 55° C., and the temperature is maintained for 24 hours, then cooled to normal temperature, and then 500 ppm of hydrogen benzophenone (hydrobenzophenone) is added as a polymerization inhibitor to obtain a solid content of 30% by weight. of polymers.
[0084] In order to remove unreacted monomers in the polymer solution, 100 parts by weight of the polymer solution were precipitated with respect to 1000 parts by weight of n-hexane. A...
Embodiment 1
[0086] Embodiment 1 (preparation of negative photosensitive resin composition)
[0087] 100 parts by weight of the acrylic copolymer solution prepared in Synthesis Example 1, 20 parts by weight of a photoinitiator represented by the following chemical formula 4, and 5 parts by weight of a urethane acrylate oligomer having 10 functional groups were mixed. 20 parts by weight of dipentaerythritol hexaacrylate as a polyfunctional monomer having an ethylenically unsaturated bond, 3 parts by weight of a melamine crosslinking agent represented by the following chemical formula 5, and (3-shrinkage Glyceryloxypropyl) methyldiethoxysilane 2 parts by weight. After adding and dissolving propylene glycol methyl ether acetate to the mixture so that the solid content would be 20% by weight, it was filtered through a 0.2-μm micromesh filter to prepare a photosensitive resin composition coating solution.
[0088] [chemical formula 4]
[0089]
[0090] [chemical formula 5]
[0091]
[...
Embodiment 2
[0093] Embodiment 2 (preparation of negative photosensitive resin composition)
[0094] A photosensitive resin composition coating solution was prepared using the same method as in Example 1, except that a photoinitiator represented by the following Chemical Formula 6 was used instead of the photoinitiator represented by Chemical Formula 4 in Example 1.
[0095] [chemical formula 6]
[0096]
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