for si 3 no 4 Ceramic surface metallization material and preparation method and brazing process
A ceramic surface and metallization technology, applied in the direction of welding/cutting media/materials, metal processing equipment, manufacturing tools, etc., can solve the problems of limited use range, joint strength drop, ceramic cracking, etc., to improve wettability, reduce Small stress concentration, strong adhesion effect
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Embodiment 1
[0035] The composition and mass percentage ratio of the solder cladding material are: Cu21%, Ti3.5%, Ni2.3%, Ce0.25%, Sc0.28%, Re0.58%, and the rest is Ag; The composition and particle size are: 40 μm for Ag, Cu, Ti and Ni, 25 μm for Ce, Sc and Re; the thickness of the Ag-based material is 400 μm.
[0036] One for Si 3 N 4 The preparation method of the silver base material metal cloth of ceramic surface metallization comprises the following steps:
[0037] (1) Weigh Ag, Cu, Ti, Ni, Ce, Sc and Re powder, and mix it;
[0038] (2) Put the mixed metal powder particles into the automatic stirring equipment container, and add a kind of adhesive, then close the container, and get a uniform mixture after fully stirring, wherein the volume ratio of the mixed metal powder particles to the adhesive is 5 :1;
[0039] (3) Under normal temperature conditions, the mixture obtained in step 2 is vacuum stirred by automatic mixing and stirring equipment, and the stirring time is 3 hours, s...
Embodiment 2
[0050] The composition and mass percentage ratio of the solder cladding material are: Cu22.5%, Ti4%, Ni2.5%, Ce0.2%, Sc0.25%, Re0.55%, and the rest is Ag; The composition and particle size are: 50 μm for Ag, Cu, Ti and Ni, 20 μm for Ce, Sc and Re; the thickness of the Ag-based material is 500 μm.
[0051] One for Si 3 N 4 The preparation method of the silver base material metal cloth of ceramic surface metallization comprises the following steps:
[0052] (1) Weigh Ag, Cu, Ti, Ni, Ce, Sc and Re powder, and mix it;
[0053] (2) Put the mixed metal powder particles into the automatic stirring equipment container, and add a kind of adhesive, then close the container, and get a uniform mixture after fully stirring, wherein the volume ratio of the mixed metal powder particles to the adhesive is 5 :1;
[0054] (3) Under normal temperature conditions, the mixture obtained in step 2 is vacuum stirred by automatic mixing and stirring equipment, and the stirring time is 2 hours, so...
Embodiment 3
[0065] The composition and mass percentage ratio of the solder cladding material are: Cu20%, Ti3%, Ni2%, Ce0.1%, Sc0.2%, Re0.5%, and the rest is Ag; the composition and particle size of the silver-based material For: 55 μm for Ag, Cu, Ti and Ni, 20 μm for Ce, Sc and Re; thickness of Ag-based material is 450 μm.
[0066] One for Si 3 N 4 The preparation method of the silver base material metal cloth of ceramic surface metallization comprises the following steps:
[0067] (1) Weigh Ag, Cu, Ti, Ni, Ce, Sc and Re powders by Cu20%, Ti3%, Ni2%, Ce0.1%, Sc0.2%, Re0.5%, Ag74.2%, and mix it up;
[0068] (2) Put the mixed metal powder particles into the automatic stirring equipment container, and add a kind of adhesive, then close the container, and get a uniform mixture after fully stirring, wherein the volume ratio of the mixed metal powder particles to the adhesive is 5 :1;
[0069] (3) Under normal temperature conditions, the mixture obtained in step 2 is vacuum stirred by auto...
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