Fusion protein for detection of anti-porcine enterotoxigenic Escherichia coli antibody, preparation method and application
A technology of fusion protein and Escherichia coli, applied in chemical instruments and methods, using vectors to introduce foreign genetic material, bacteria, etc., can solve the problems of complicated adhesin purification methods, easy cross-reaction, low purity and yield, etc., to achieve immunity Good reactivity, low cost, and high yield
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Embodiment 1
[0022] Example 1 Preparation of fusion protein for detection of anti-ETEC antibodies
[0023] 1. Fusion gene designed to detect anti-ETEC antibody
[0024] The nucleotide and amino acid sequences of ETEC F4(K88) pili and ETEC F5(K99) pili were analyzed by the biological software DNAStar. After analysis using the codon optimization software CodonAdaptationTool (JCAT), the rare codons of E. coli in the nucleotide sequences of F4 and F5 pili were replaced with preferred codons, and a linker sequence was added between the gene fragments of F4 and F5 pili. The fusion gene was designed, and its sequence is shown in SEQ ID NO:2. Add an EcoRI restriction site at the 5' end of the fusion gene, add a Sal I restriction site at the 3' end, and send it to Nanjing GenScript Biotechnology Company for synthesis.
[0025] The fusion genes encode fusion proteins F4-F5 for detection of anti-ETEC antibodies. The amino acid sequence of the fusion protein F4-F5 is shown in SEQ ID NO:1.
[0026]...
Embodiment 2
[0039] Embodiment 2 Detects the composition and method of use of the anti-ETEC antibody kit
[0040] 1. The composition of the kit
[0041] 1. Washing solution: prepare pH 7.4, 0.01M phosphate buffer solution, and add Tween-20 with a final concentration of 0.05%. Specific preparation method: weigh KH 2 PO 4 0.2g, Na 2 HPO 4 12H 2 Dissolve 2.9g of O and 8g of NaCl in water, then dilute to 1000mL, and add 0.5mL of Tween-20.
[0042] 2. Diluent: pH7.4, 0.01M phosphate buffer, the preparation method is the same as above.
[0043] 3. Stop solution: 2M sulfuric acid solution, dilute 111.2mL of concentrated sulfuric acid with water and dilute to 1000mL.
[0044] 4. Substrate chromogenic solution: soluble TMB one-component substrate chromogenic solution (purchased from Nanjing Zhuyan Biotechnology Co., Ltd.).
[0045] TMB is an abbreviation for 3,3’,5,5’-tetramethylbenzidine.
[0046] 5. ETEC-positive serum standard product: from multiple ETEC-immunized piglet sera, select a ...
Embodiment 3
[0080] Embodiment 3 specificity experiment
[0081] Investigate the specificity of the kit in Example 2. Adopt kit in embodiment 2 to know PEDV (porcine epidemic diarrhea virus), PRRSV (porcine reproductive and respiratory syndrome virus), PRV (pseudorabies virus), CSFV (swine fever virus), PCV2 with indirect ELISA method (Porcine circovirus type 2), APP (Actinobacillus pleuropneumoniae) and SS (Streptococcus suis) positive sera were tested. Three parallel replicates were performed for each serum. The OD value of each well was measured with a microplate reader at a wavelength of 450 nm to determine the specificity of the indirect ELISA method. The positive sera of PEDV, PRRSV, PRV, CSFV, and PCV2 were purchased from IDEXX Company, and the positive sera of APP and SS were purchased from Wuhan Keqian Biotechnology Co., Ltd. The results showed that the S / P of PEDV, PRRSV, PRV, CSFV, FMDV, PCV2, APP, and SS positive sera were all less than 0.23, which was judged as negative.
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