Nano antimicrobial internal wall paint containing illite-montmorillonite clay and preparation method thereof
A technology of interior wall paint and smectite clay, which is applied in the field of nano-antibacterial interior wall paint and its preparation, can solve problems such as unstable product quality, pollution and damage, and loss of protective effect of the coating, and achieve excellent anti-fungal performance and good compatibility. Capacitive, anti-fungal properties for long-lasting effectiveness
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Embodiment 1
[0037] (1) Dry crushing: mechanically crushing the natural imonite clay mineral into imonite mixed layer clay ore fragments with a particle size of less than 5cm;
[0038] (2) Soaking: 450g of Imono mixed-layer clay ore fritters and 550g of water are mixed, then soaked for 12h to obtain Yimeng clay slurry;
[0039] (3) Ramping: use 0.1mol / L NaOH solution to adjust the pH value of the Iraqi / Mongolian clay slurry to 9, add 6.75g dispersant WF-211, and use a sand mill disperser to ram and disperse; wherein, dispersing The addition of agent WF-211 is 1.5wt% of the solid content in the slurry; the rotating speed of the sand mill disperser is 1000rpm, and the stirring time is 30min;
[0040] (4) Screening: the slurry after step (3) pounding and dispersing is passed through a 500 mesh sieve to obtain the slurry under the sieve;
[0041] (5) Iron removal: adopt high gradient magnetic separator to carry out iron removal to the slurry that step (4) obtains, and slurry circulates 3 time...
Embodiment 2
[0046] The difference between this embodiment and Example 1 is: the grinding time in step (7) is 24h, and the particle cumulative distribution figure of the slurry is as follows figure 1 As shown in the 24h curve in the middle, it can be seen that the particles less than 100nm account for about 55%, and the particle size reaches the nanoscale; in the step (8), get the water-based interior wall of the Yimeng clay nano-slurry of 75g and 425g pure acrylate copolymer emulsion system The latex paint is placed in a beaker and mixed to prepare a nano antibacterial interior wall paint containing 15 wt% of the Imon clay nano slurry.
Embodiment 3
[0048] The difference between this embodiment and Example 1 is: the grinding time in step (7) is 48h, and the particle cumulative distribution figure of the slurry is as follows figure 1 As shown in the 48h curve in the middle, it can be seen that the particles less than 100nm account for about 73%, and the particle size reaches the nanoscale; in step (8), get the water-based interior wall of the Yimeng clay nano slurry of 100g and 400g pure acrylate copolymer emulsion system The latex paint is placed in a beaker and mixed to prepare a nano-antibacterial interior wall paint containing 20 wt% of the Imon clay nano-slurry.
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